


卷 42, 编号 1 (2016)
- 年: 2016
- 文章: 30
- URL: https://bakhtiniada.ru/1063-7850/issue/view/12304
Article
Obtaining of crystals of polyelemental solid solutions of rare earth hexaborides
摘要
Single crystals of polyelemental rare earth hexaborides with the preset formula La0.5(Ce0.1Pr0.1Nd0.1Sm0.1Eu0.1)B6 were obtained for the first time. Synthesis and crystallization were performed by the solution–melt method in an immiscible Al/Pb system. Step-by-step chemical analysis was made with the aid of a CAMEBAX microprobe. The inclusion of all rare earth metals (REMs) in the hexaboride lattice was proven, and differences in the composition of obtained crystals caused by nonstationarity of the bulk crystallization process were found. The lattice periods of the polyelemental REM hexaborides were found to be smaller than that of hexaboride of lanthanum, the main element of the metal sublattice. The measured microhardness of the new material lies within the range of the microhardness values of hexaborides of all its constituent REMs. Speculations are provided on the peculiarities of the growth mechanism, crystallization, and composition of the obtained crystals.



YBa2Cu3O7–δ-based ceramic materials manufactured from nanopowders
摘要
The results of studying the structure and electrical resistance of nanostructured YBa2Cu3O7–δ-based superconducting ceramics of various density optimally saturated by oxygen and fabricated from nanopowders are given.



Radiation and dynamics of a nanoparticle in equilibrium background radiation upon translational–rotational motion
摘要
We have obtained general expressions for the intensity of radiation and tangential force of a small polarizable particle in the process of translational–rotational motion in equilibrium radiation background (thermalized photon gas) of a certain temperature at an arbitrary relative orientation of the linear and angular velocity vectors. It is shown that, in a cold vacuum background, the translational velocity of particle is independent of time and the intensity of its spontaneous emission is determined by the angular velocity and imaginary part of the particle polarizability.



Signals of an intermodal fiber interferometer induced by laser frequency modulation
摘要
Signals of an intermodal fiber interferometer induced by laser optical frequency modulation are studied. Dependences of signal amplitudes and spectra on the laser frequency deviation are examined theoretically and experimentally for various optical fibers. It is established that the sensitivity of the intermodal fiber interferometer to the laser frequency variation essentially depends on the fiber refractive index profile. The minimal sensitivity corresponds to graded-index (α ≈ 2) multimode optical fibers. Step-index optical fibers (α = ∞) are more sensitive to the laser frequency variation by more than a factor of 100.



Boundaries of the ambiguity area upon reflection of compression shock waves
摘要
Oblique shock waves can be reflected from hard walls, the axis, or the plane of symmetry, as well as from other counterpropagating shock waves with the formation of regular and Mach shock wave configurations. The specific form of shock wave structures is determined by the parameters of the problem: Mach number and intensity of incident shock waves. On the plane of parameters, there exists an ambiguity area in which laws of conservation admit both the regular and Mach reflection of shock waves. The boundaries of this region have been determined.



Thermal lithography of thin films of vanadium dioxide
摘要
A technique is proposed for making microareas with sharply different optical and electrical properties in thin films of vanadium dioxide. The technique is based on vacuum annealing of thin films, which results in a yield of oxygen from vanadium dioxide with the formation of an oxygen vacancy in it.



A heterojunction photovoltaic cell based on a mixture of silane copolymer with C70 fullerene derivative
摘要
Heterojunction photovoltaic cells with a photoactive layer composed of a mixture of a silane copolymer with a fullerene derivative PC70BM have been fabricated, and their working characteristics have been measured. Data obtained by cyclic voltammetry were used to construct the energy level diagram for the cell components. Analysis of the diagram and photoelectric characteristics of the photovoltaic cell made it possible to find ways to improve its efficiency.



Wave spectrum of a conducting cylinder in an isotropic plasma
摘要
The boundary value problem of the propagation of an electromagnetic field along a cylindrical conductor in an isotropic plasma medium has been solved by the impedance method. The boundedness of the wave spectrum of such a guiding structure has been shown. The spectrum includes fast intrinsic wave E01 and extrinsic hybrid waves HEnm and EHnm, both fast and slow ones, their countable set being determined by the azimuthal index.



Modification of the properties of vanadium dioxide by plasma-immersion ion implantation
摘要
The effect of hydrogenation of thin films of vanadium dioxide by plasma-immersion ion implantation on their conductivity is characterized. It is demonstrated that the parameters of the metal–insulator phase transition observed in VO2 films depend on the irradiation dose. If the dose exceeds a certain threshold, film metallization occurs and the phase transition vanishes. The time of retention of hydrogen within films is considerably longer than that typical for other hydrogenation methods.



Forming dense arrays of gold nanoparticles in thin films of yttria stabilized zirconia by magnetron sputtering
摘要
Layers of Au nanoparticles (NPs) were formed in films of yttria stabilized zirconia (YSZ) on fusedquartz substrates by layer-by-layer magnetron deposition with subsequent annealing. The obtained structures were studied by applying high-resolution transmission electron microscopy (TEM) to transverse sections and using optical absorption spectroscopy. TEM studies revealed the formation of Au NPs with a diameter of 2?3 nm concentrated in a thin layer within the YSZ film. The optical absorption spectra of the studied samples exhibited peaks of resonance plasmon absorption in Au NPs with a maximum wavelength of ~650 nm. The dependences of geometric and structural parameters of Au NP arrays (size, density, thickness of the Au NP layer, etc.) on the formation conditions were determined, and the regimes of fabrication of dense Au NP arrays that allow for collective plasmon excitations were identified.



Amplification of plasma waves in shielded active graphene
摘要
Amplification of plasma waves in shielded graphene with inverted energy distribution of charge carriers is investigated theoretically. It is shown that graphene shielding allows one to increase an amplification factor of terahertz plasmons in several times compared to the case of amplification of unshielded plasmons due to strong field confinement of the shielded plasmons near graphene.



Parameters of silicon carbide diode avalanche shapers for the picosecond range
摘要
Parameters of ultrafast avalanche switching of high-voltage diode structures based on 4H-SiC have been estimated theoretically. The calculation was carried out using the analytical theory of the impact ionization wave of the TRAPATT type, which makes it possible to determine the main characteristics of a wave for arbitrary dependences of the impact ionization coefficients and carrier drift velocity on electric field. It is shown that, for a high-voltage (1–10 kV) 4H-SiC structure, the time of switching from the blocking to the conducting state is ~10 ps, which is an order of magnitude shorter than that for a Si structure with the same stationary breakdown voltage, and the concentration of the electron-hole plasma created by the wave is two orders of magnitude higher. Picosecond switching times can be reached for 4H-SiC structures with a stationary breakdown voltage exceeding 10 kV.



Determination of the coupling architecture and parameters of elements in ensembles of time-delay systems
摘要
A method for the reconstruction of the architecture, strength of couplings, and parameters of elements in ensembles of coupled time-delay systems from their time series is proposed. The effectiveness of the method is demonstrated on chaotic time series of the ensemble of diffusively coupled nonidentical Ikeda equations in the presence of noise.



Grain boundary engineering and superstrength of nanocrystals
摘要
A new paradigm of hardening of nanocrystals is proposed based on the competing influence of various mechanisms of plastic deformation, i.e., dislocation sliding and grain-boundary slip. It has been confirmed using the results of computer modeling and the experimental data that the use of grain boundary engineering on the basis of the proposed ideas makes it possible to enhance substantially the strength of titaniumbased materials up to ultimate (theoretical) values.



Energy model of radial growth of a nanotubular crystal
摘要
An energy model of the formation of multiwall nanoscrolls from thin layers is proposed. It is established that the radial growth of a nanoscroll can be accompanied by variation of the ratio of its internal and external diameters. The influence of the main physical parameters of the model on this ratio is considered.



NMR study of domain wall pinning in a magnetically ordered material
摘要
The use of nuclear magnetic resonance in the form of spin echo in combination with magnetic field pulses applied to a magnetically ordered material sample offers a convenient tool for studying characteristics of the centers of domain-wall pinning. Possibilities of this method have been demonstrated in experiments with lithium–zinc ferrite.



PIV analysis of the homogeneity of energy deposition during development of a plasma actuator channel
摘要
Nonstationary velocity fields that arise during the development of flows behind shock (blast) waves initiated by pulsed surface sliding discharge in air at a pressure of (2–4) × 104 Pa have been experimentally studied by the particle image velocimetry (PIV) technique. Plasma sheets (nanosecond discharges slipping over a dielectric surface) were initiated on walls of a rectangular chamber. Spatial analysis of the shape of shock-wave fronts and the distribution of flow velocities behind these waves showed that the pulsed energy deposition is homogeneous along discharge channels of a plasma sheet, while the integral visible plasma glow intensity decreases in the direction of channel propagation.



The effect of external stresses on the behavior of photoacoustic signals inside vickers indenter marks on a steel surface
摘要
It is experimentally established that the characteristics of photoacoustic signals inside Vickers indenter marks in metals significantly change under the action of external stresses. Relative changes in the signal amplitude are estimated in the framework of a quasi-static approximation based on the temperature dependence of the elastic modulus of the metal.



A magnetosensitive thin-film silicon Hall-type field-effect transistor with operating temperature range expanded up to 350°C
摘要
We describe a magnetosensitive device consisting of a combination of a thin-film Si transistor with built-in conducting channel (fabricated by the silicon-on-insulator technology) and a Hall-type sensor (HS). The transistor has a double-gate field control system of the metal–insulator–semiconductor–insulator–metal type and operates in the regime of carrier accumulation in the channel at partial depletion of adjacent regions of the Si film. It is established that the device can operate at temperatures up to about 350°C, which is 160–180°C higher than the maximum operating temperature of HSs based on bulk Si crystals and comparable with HSs based on wide-bandgap semiconductors.



Thermoelastic martensitic transformations in ternary Ni50Mn50–zGaz alloys
摘要
We have studied the effect of gallium alloying on the structure, phase composition, and physical properties of ternary alloys of the Ni50Mn50–zGaz (0 ≤ z ≤ 25 at %) quasi-binary section in a broad temperature range. Dependences of the type of crystalline structure of the high-temperature austenite phase and martensite, as well as the critical temperatures of martensitic transformations on the alloy composition, are determined. A phase diagram of the structural and magnetic transformations is constructed. Concentration boundaries of the existence of tetragonal L10 (2M) martensite and martensitic phases (10M and 14M) with complex multilayer crystalline lattices are found. It is established that the predominant martensite morphology is determined by the hierarchy of packets of thin coherent nano- and submicrocrystalline plates with habit planes close to {011}B2, pairwise twinned along one of 24 equivalent {011}<011>B2 twinning shear systems.



A high-power low-temperature air plasma generator with a divergent channel of the output electrode
摘要
We have developed and studied a powerful high-enthalpy (H ≥ 20 kJ/g) air plasma jet generator with a divergent channel of the output electrode, which belongs to the class of dc plasmatrons with a thermionic cathode. The plasma generator possesses an efficiency of about 80% and ensures the formation of slightly divergent (2± = 12°) plasma jet with diameter D = 50 mm and a mass-average temperature of 6000–9000 K.



Wavelet filtration of noisy images
摘要
Methods of noisy image filtration using wavelet transforms with real and complex basis sets have been compared. It is shown that the use of a complex wavelet transform provides more effective filtration and admits automatic optimization of the filter parameters. Optimized choice of the threshold level during filtration based on a complex wavelet transform significantly decreases the error of image reconstruction as compared to that achieved with a standard method of discrete wavelet transform employing basis sets of the Daubechies wavelet family.



Spin polarization of 85Rb atoms in collisions with optically oriented metastable 4He atoms in alkali–helium plasma
摘要
We have experimentally detected a signal of magnetic resonance (MR) from 85Rb atoms in the 52S1/2 state by measuring the absorption of light from a helium lamp producing optical orientation of metastable 23S14He atoms in a cell containing alkali metal vapor and gaseous helium at a pressure of 1 Torr. The ratio of MR signal amplitudes in Rb and He atoms did not exceed 10–2. Peculiarities of the formation and observation of the collisional polarization of Rb atoms in alkali–helium plasma are discussed.



Nonlinear room-temperature Hall effect in n-InFeAs layers
摘要
Ferromagnetic n-InFeAs layers have been obtained by the method of laser ablation in vacuum. The InFeAs layers on GaAs(111) substrates exhibit nonlinear (with respect to magnetic field) Hall effect up to room temperatures. It is established that the crystallographic orientation of the GaAs substrates influences the magnetic properties of InFeAs layers.



Self-organized growth of small arrays of metal nanoislands on the surface of poled ion-exchange glasses
摘要
Self-organized metal nanostructures have been obtained by an original method on the surface of soda–lime glasses. The nanostructures are grown by heat treatment of poled glass substrates in hydrogen upon preliminary ion-exchange introduction of silver. The poling is produced with the aid of a profiled anode electrode. Using the proposed method, it is possible to grow separate metal nanoislands and ordered nanostructures of several islands on the glass surface. The islands are formed in submicron-sized unpoled regions as a result of self-assembly during out-diffusion of silver. Minimum spacing in linear groups of two or three silver islands is 20–30 nm at their characteristic size of about 100 nm. The proposed method allows nanoisland arrays and groups of a few islands to be grown and multiplicated.



InAs/GaSb superlattices fabricated by metalorganic chemical vapor deposition
摘要
The possibility of fabricating InAs/GaSb strained-layer superlattices by metalorganic chemical vapor deposition has been experimentally demonstrated. The results of transmission electron microscopy and photoluminescence spectroscopy investigations showed that the obtained structures comprise an InAs?GaSb superlattice on a GaSb substrate consisting of 2-nm-thick InAs and 3.3-nm-thick GaSb layers.



Sensitivity of experiment on search for neutron–antineutron oscillations on the projected ultracold neutron source at the WWR-M reactor
摘要
An experiment on search for neutron–antineutron oscillations is proposed based on the storage of ultracold neutrons (UCNs) in a material trap. The main factors influencing sensitivity of the experiment are the trap size and the amount of UCNs trapped. A high-intensity UCN source will be created at the WWR-M reactor of Petersburg Nuclear Physics Institute, which must provide an UCN density two to three orders of magnitude higher than that in the existing sources. The results of simulations of the experiment for detecting neutron–antineutron oscillations with the new source show that the sensitivity can be increased by ~20–80 times compared to existing depending on the model of neutron reflection from walls.



Dispersed state of C60 fullerene in some polymers
摘要
The character of C60 fullerene dispersion and its temperature dependence in various polymer matrices has been studied by UV-Vis spectroscopy and thermodesorption mass spectrometry. It is established that the degree of fullerene aggregation in these composites varies from molecular-dispersed state to largesize clusters. For the polymers studied, the initial dispersed state is most stable with respect to temperature in the case of poly-α-methylstyrene.



Mechanical properties of (Bi,Sb)2Te3 solid solutions obtained by directional crystallization and spark plasma sintering
摘要
We have studied the temperature dependence of the mechanical strength at uniaxial compression for solid solutions based on bismuth and antimony chalcogenides, which were prepared by three methods: (i) vertical zone melting (VZM), (ii) hot extrusion, and (iii) spark plasma sintering (SPS). In the samples of solid solutions obtained by VZM and extrusion, a brittle–ductile transition was observed in a wised temperature interval of 200–350°C. In nanostructured SPS samples, transition from brittle to plastic fracture was observed within 170–200°C. The room-temperature strength of nanostructured samples was eight to nine times as large as that of VZM samples, and the stress–strain curves of these materials were significantly different. At a temperature of about 300°C, the strength of nanostructured solid solutions decreases to nearly zero.



Possible observation of the isotope effect during field evaporation
摘要
The field evaporation of tungsten at high temperatures (T ~ 2000 K) has been studied using a magnetic mass spectrometer equipped with a field ion source. Only low-charge ions (W+2 and W+) have been observed in the course of evaporation for all tungsten isotopes. For singly charged ions only, the number of ions of the heaviest isotope, 186W+, was about one order of magnitude lower than that corresponding to the standard isotope ratio for natural tungsten. An explanation of this anomalous phenomenon is proposed.


