Catalytic thiomethylation of N-substituted ureas and thioureas with N,N,N′,N′-tetramethylmethanediamine and α,ω-alkanedithiols


Cite item

Full Text

Open Access Open Access
Restricted Access Access granted
Restricted Access Subscription Access

Abstract

An efficient procedure has been developed for the synthesis of N,N′-(2,5-dithiaalkane-α,ω-diyl)bis-(N′-allylthioureas) by thiomethylation of N-substituted ureas and thioureas with α,ω-alkanedithiols and N,N,N′,N′-tetramethylmethanediamine in the presence of cesium carbonate as catalyst.

About the authors

R. R. Khairullina

Institute of Petrochemistry and Catalysis

Author for correspondence.
Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, Bashkortostan, 450075

A. R. Geniyatova

Institute of Petrochemistry and Catalysis

Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, Bashkortostan, 450075

E. S. Meshcheryakova

Institute of Petrochemistry and Catalysis

Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, Bashkortostan, 450075

T. V. Tyumkina

Institute of Petrochemistry and Catalysis

Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, Bashkortostan, 450075

L. M. Khalilov

Institute of Petrochemistry and Catalysis

Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, Bashkortostan, 450075

A. G. Ibragimov

Institute of Petrochemistry and Catalysis

Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, Bashkortostan, 450075

U. M. Dzhemilev

Institute of Petrochemistry and Catalysis

Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, Bashkortostan, 450075

Supplementary files

Supplementary Files
Action
1. JATS XML

Copyright (c) 2017 Pleiades Publishing, Ltd.