Synthesis of  N -aryl-2-methyl-4-oxo-3,4,5,6-tetrahydro-2 H -2,6-methano-1,3,5-benzoxadiazocine-11-carboxamides

V. L. Gein; T. M. Zamaraeva; M. V. Dmitriev; O. E. Nasakin

doi:10.1134/S1070428017060094

Synthesis of N-aryl-2-methyl-4-oxo-3,4,5,6-tetrahydro-2H-2,6-methano-1,3,5-benzoxadiazocine-11-carboxamides

作者: Gein V.L.¹, Zamaraeva T.M.¹, Dmitriev M.V.², Nasakin O.E.³
隶属关系:
1. Perm State Pharmaceutical Academy
2. Perm State National Research University
3. I.N. Ul’yanov Chuvash State University
期: 卷 53, 编号 6 (2017)
页面: 869-872
栏目: Article
URL: https://bakhtiniada.ru/1070-4280/article/view/216350
DOI: https://doi.org/10.1134/S1070428017060094
ID: 216350

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详细

N-Aryl-2-methyl-4-oxo-3,4,5,6-tetrahydro-2H-2,6-methano-1,3,5-benzoxadiazocine-11-carboxamides were synthesized by three-component reactions of N-aryl-3-oxobutanamides with salicylaldehyde and urea in ethanol in the presence of NaHSO₄ as catalyst. The product structure was determined by IR and ¹H NMR spectroscopy and X-ray analysis.