Отправить статью по E-mail Asymmetric Ir-catalyzed hydrogenation of 1,3-dihydro-2H-1,5-benzodiazepin-2-ones using phosphoramidites
- Авторы: Sokolovskaya M.V.1, Lyubimov S.E.1, Mikhel I.S.2, Birin K.P.2, Davankov V.A.1
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Учреждения:
- A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences
- A. N. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
- Выпуск: Том 67, № 2 (2018)
- Страницы: 260-264
- Раздел: Full Articles
- URL: https://bakhtiniada.ru/1066-5285/article/view/242116
- DOI: https://doi.org/10.1007/s11172-018-2068-9
- ID: 242116
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Аннотация
A series of phosphoramidite ligands was tested in the asymmetric hydrogenation of 4-arylsubstituted 1,3-dihydro-2H-benzodiazepine-2-ones and up to 52% ee was achieved. The effects of various factors (solvents, hydrogen pressure, and addition of phosphine ligands) on the hydrogenation were studied.
Об авторах
M. Sokolovskaya
A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences
Email: lssp452@mail.ru
Россия, 28 ul. Vavilova, Moscow, 119991
S. Lyubimov
A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences
Автор, ответственный за переписку.
Email: lssp452@mail.ru
Россия, 28 ul. Vavilova, Moscow, 119991
I. Mikhel
A. N. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
Email: lssp452@mail.ru
Россия, 31/4 Leninsky prosp., Moscow, 119071
K. Birin
A. N. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
Email: lssp452@mail.ru
Россия, 31/4 Leninsky prosp., Moscow, 119071
V. Davankov
A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences
Email: lssp452@mail.ru
Россия, 28 ul. Vavilova, Moscow, 119991
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