Study of Kinetics of Solid Phase Transition in Tetracosane С 24 Н 50  by High-Resolution Synchrotron X-Ray Powder Diffraction

V. A. Marikhin; P. V. Dorovatovskii; Ya. V. Zubavichus; M. V. Baidakova; E. M. Ivan’kova; L. P. Myasnikova

doi:10.1134/S1063783419060106

Study of Kinetics of Solid Phase Transition in Tetracosane С₂₄Н₅₀ by High-Resolution Synchrotron X-Ray Powder Diffraction

作者: Marikhin V.A.¹, Dorovatovskii P.V.², Zubavichus Y.V.³, Baidakova M.V.¹, Ivan’kova E.M.⁴, Myasnikova L.P.¹
隶属关系:
1. Ioffe Institute
2. National Research Center Kurchatov Institute
3. Boreskov Institute of Catalysis, Siberian Branch of the Russian Academy of Sciences
4. Institute of High-Molecular Compounds, Russian Academy of Sciences
期: 卷 61, 编号 6 (2019)
页面: 1128-1135
栏目: Polymers
URL: https://bakhtiniada.ru/1063-7834/article/view/205818
DOI: https://doi.org/10.1134/S1063783419060106
ID: 205818

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Using the small-angle synchrotron X-ray diffraction method at the research facility “BELOK” of the Kurchatov synchrotron radiation source at the NRC Kurchatov Institute, it was shown that the first-order solid phase transition in tetracosane C₂₄H₅₀ passes according to a heterogeneous mechanism in a narrow temperature range ΔT ~ 1 K in accordance with the theory of diffuse phase transitions.