Enviar artigo por via de e-mail Influence of the composition of [Ti(OC4H9)4 – x(O2C5H7)x] complexes and hydrolysis conditions on the synthesis of titania by sol–gel technology
- Autores: Simonenko N.P.1, Nikolaev V.A.1, Simonenko E.P.1,2, Sevastyanov V.G.1,2, Kuznetsov N.T.1,2
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Afiliações:
- Kurnakov Institute of General and Inorganic Chemistry
- Samara State Aerospace University (National Research University)
- Edição: Volume 61, Nº 8 (2016)
- Páginas: 929-939
- Seção: Synthesis and Properties of Inorganic Compounds
- URL: https://bakhtiniada.ru/0036-0236/article/view/166659
- DOI: https://doi.org/10.1134/S0036023616080167
- ID: 166659
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Resumo
The influence of the coordination sphere of [Ti(OC4H9)4–x(O2C5H7)x] complexes, concentration in solution, and the ratio n(H2O)/n(Ti4+) on the hydrolysis and polycondensation kinetics of the complexes, the stability of the resulting gels, the thermal behavior of then-formed xerogels, the shift of anatase–rutile phase transition temperature, and the microstructure of the product, was determined.
Sobre autores
N. Simonenko
Kurnakov Institute of General and Inorganic Chemistry
Autor responsável pela correspondência
Email: n_simonenko@mail.ru
Rússia, Leninskii pr. 31, Moscow, 119991
V. Nikolaev
Kurnakov Institute of General and Inorganic Chemistry
Email: n_simonenko@mail.ru
Rússia, Leninskii pr. 31, Moscow, 119991
E. Simonenko
Kurnakov Institute of General and Inorganic Chemistry; Samara State Aerospace University (National Research University)
Email: n_simonenko@mail.ru
Rússia, Leninskii pr. 31, Moscow, 119991; Samara
V. Sevastyanov
Kurnakov Institute of General and Inorganic Chemistry; Samara State Aerospace University (National Research University)
Email: n_simonenko@mail.ru
Rússia, Leninskii pr. 31, Moscow, 119991; Samara
N. Kuznetsov
Kurnakov Institute of General and Inorganic Chemistry; Samara State Aerospace University (National Research University)
Email: n_simonenko@mail.ru
Rússia, Leninskii pr. 31, Moscow, 119991; Samara
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