电邮这篇文章 Thermal decomposition of cerium(III) perchlorate
- 作者: Skogareva L.S.1, Baranchikov A.E.1,2, Shekunova T.O.2, Ivanov V.K.1,3
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隶属关系:
- Kurnakov Institute of General and Inorganic Chemistry
- Moscow State University
- Tomsk State University
- 期: 卷 61, 编号 8 (2016)
- 页面: 1019-1025
- 栏目: Physical Methods of Investigation
- URL: https://bakhtiniada.ru/0036-0236/article/view/166697
- DOI: https://doi.org/10.1134/S0036023616080180
- ID: 166697
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详细
Thermal decomposition of Ce(ClO4)3 • 9H2O and Ce(ClO4)3 to give cerium(IV) dioxide in the temperature range 240–460°C was studied by DSC–TGA, X-ray powder diffraction, IR and mass spectroscopy. The thermolysis of these salts was shown to proceed through the stage of formation of intermediate product supposedly cerium oxoperchlorate. The thermal decomposition of cerium(III) perchlorate hydrate at 460°C leads to formation of nanocrystalline cerium dioxide with particle size of 13 nm.
作者简介
L. Skogareva
Kurnakov Institute of General and Inorganic Chemistry
编辑信件的主要联系方式.
Email: skog@igic.ras.ru
俄罗斯联邦, Leninskii pr. 31, Moscow, 119991
A. Baranchikov
Kurnakov Institute of General and Inorganic Chemistry; Moscow State University
Email: skog@igic.ras.ru
俄罗斯联邦, Leninskii pr. 31, Moscow, 119991; Moscow, 119991
T. Shekunova
Moscow State University
Email: skog@igic.ras.ru
俄罗斯联邦, Moscow, 119991
V. Ivanov
Kurnakov Institute of General and Inorganic Chemistry; Tomsk State University
Email: skog@igic.ras.ru
俄罗斯联邦, Leninskii pr. 31, Moscow, 119991; pr. Lenina 36, Tomsk, 634050
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