Мақаланы E-mail арқылы жіберу Thermal decomposition of cerium(III) perchlorate
- Авторлар: Skogareva L.S.1, Baranchikov A.E.1,2, Shekunova T.O.2, Ivanov V.K.1,3
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Мекемелер:
- Kurnakov Institute of General and Inorganic Chemistry
- Moscow State University
- Tomsk State University
- Шығарылым: Том 61, № 8 (2016)
- Беттер: 1019-1025
- Бөлім: Physical Methods of Investigation
- URL: https://bakhtiniada.ru/0036-0236/article/view/166697
- DOI: https://doi.org/10.1134/S0036023616080180
- ID: 166697
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Аннотация
Thermal decomposition of Ce(ClO4)3 • 9H2O and Ce(ClO4)3 to give cerium(IV) dioxide in the temperature range 240–460°C was studied by DSC–TGA, X-ray powder diffraction, IR and mass spectroscopy. The thermolysis of these salts was shown to proceed through the stage of formation of intermediate product supposedly cerium oxoperchlorate. The thermal decomposition of cerium(III) perchlorate hydrate at 460°C leads to formation of nanocrystalline cerium dioxide with particle size of 13 nm.
Авторлар туралы
L. Skogareva
Kurnakov Institute of General and Inorganic Chemistry
Хат алмасуға жауапты Автор.
Email: skog@igic.ras.ru
Ресей, Leninskii pr. 31, Moscow, 119991
A. Baranchikov
Kurnakov Institute of General and Inorganic Chemistry; Moscow State University
Email: skog@igic.ras.ru
Ресей, Leninskii pr. 31, Moscow, 119991; Moscow, 119991
T. Shekunova
Moscow State University
Email: skog@igic.ras.ru
Ресей, Moscow, 119991
V. Ivanov
Kurnakov Institute of General and Inorganic Chemistry; Tomsk State University
Email: skog@igic.ras.ru
Ресей, Leninskii pr. 31, Moscow, 119991; pr. Lenina 36, Tomsk, 634050
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