Plane-Parallel Microvolume Cells for Studying the Structure of Solutions of Bioorganic Strongly Absorbing and Weakly Scattering Objects at the BioSAX Beamline of Kurchatov Synchrotron Radiation Source

Мұқаба

Дәйексөз келтіру

Толық мәтін

Аннотация

Microvolume cells for studying the structure of solutions by the SAXS method using synchrotron radiation have been designed and created. The cells were tested at the BioMUR station of the Kurchatov synchrotron radiation source. A comparative analysis of two-dimensional small-angle scattering patterns from a standard capillary and from the developed cells has been carried out, which showed a significant improvement in the quality of SAXS experimental data without the need to complicate the data processing procedure when using cells instead of capillaries. The possibility of studying strongly absorbing and weakly scattering samples, as well as the dynamics of SAXS scattering curves for solutions is shown.

Авторлар туралы

Andrei Sukhanov

NRC “Kurchatov Institute”

Хат алмасуға жауапты Автор.
Email: sukhanov.ae15@physics.msu.ru
Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Vladimir Volkov

NRC “Kurchatov Institute”

Email: volkicras@mail.ru
Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Margarita Marchenkova

NRC “Kurchatov Institute”

Email: margaritkaepf@gmail.com
Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Peter Konarev

NRC “Kurchatov Institute”

Email: peter_konarev@mail.ru
Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Stanislav Paul

«Troitsk Research and Development Center» LLC

Email: paul@trdc.com
Ресей, 16, Akademik Frank Str., Moscow, Troitsk, 108840, Russia

Georgy Peters

NRC “Kurchatov Institute”

Email: georgspeters@gmail.com
Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Yury Pisarevsky

NRC “Kurchatov Institute”

Email: yupisarev@yandex.ru
Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Sergei Chapek

International Research Institute of Intelligent Materials, SFU

Email: chapek@sfedu.ru
Ресей, 178/24, Andrey Sladkov Str., Rostov-on-Don, 344090, Russia

Vladimir Shishkov

NRC “Kurchatov Institute”

Email: shiva@crys.ras.ru
Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Alexander Soldatov

International Research Institute of Intelligent Materials, SFU

Email: soldatov@sfedu.ru

Professor

Ресей, 178/24, Andrey Sladkov Str., Rostov-on-Don, 344090, Russia

Mikhail Kovalchuk

NRC “Kurchatov Institute”

Email: koval@crys.ras.ru

RAS Correspondent Member, Professor, President of NRC

Ресей, 59, Leninsky Ave., Moscow, 119333, Russia

Әдебиет тізімі

  1. A. Round, F. Felisaz, L. Fodinger, A. Gobbo, J. Huet, C. Villard, C.E. Blanchet, P. Pernot, S. McSweeney, M. Roessle, D.I. Svergun, F. Cipriani Acta Crystallogr. Sect. D Biol. Crystallogr. International Union of Crystallography, 2015, 71, 67. doi: 10.1107/S1399004714026959.
  2. G.S. Peters, Yu.A. Gaponov, P.V. Konarev, M.A. Marchenkova, K.B. Ilina, V.V. Volkov, Yu.V. Pisarevsky, M.V. Kovalchuk Nucl. Instrum. Methods Phys. Res., Sect. A, 2022, 1025, 166170. doi: 10.1016/j.nima.2021.166170.
  3. M. Hassan, S. Agraval, M. Woolley, S.M. Clarke, A. Osundare, D. Craske, R. Lindsay, A. Smith, T. Snow, T. Zinn, N. Terrill Rev. Sci. Instrum., 2023, 94(4), 043701. doi: 10.1063/5.0146013.
  4. C.J.C. Edwards-Gayle, N. Khunti, I.W. Hamley, K.Inoue, N. Cowieson, R. Rambo J. Synchtrotron Radiat., 2021, 28, 318. doi: 10.1107/S1600577520013831.
  5. N.M. Kirby, S.T. Mudie, A.M. Hawley, D.J. Cookson, H.D.T. Mertens, N. Cowieson, V. Samardzic-Boban J. Appl. Crystallogr., 2013, 46, 1670. doi: 10.1107/S002188981302774X.
  6. L.P. Cavalcanti, I.L. Torriani, T.S. Plivelic, C.L.P. Oliveira, G. Kellermann, R. Neuenschwander Rev. Sci. Intstrum., 2004, 75(11), 4541. doi: 10.1063/1.1804956.
  7. J.-M. Dubuisson, T. Decamps, P. Vachette J. Appl. Crystallogr., 1997, 30, 49. doi: 10.1107/S002188989600876X.
  8. E.G Kozyr, P.N. Njoroge, S.V. Chapek, V.V. Shapovalov, A.A. Skorynina, A.Y. Pnevskaya, A.N. Bulgakov, A.V. Soldatov, F. Pellegrino, E. Groppo, S. Bordiga, L. Mino, A.L. Bugaev Catalysts, 2023, 13, 414. doi: 10.3390/catal13020414.
  9. F. Schwemmer, C.E. Blanchet, A. Spilotros, D. Kosse, S. Zehnle, H.D.T. Mertens, M.A. Graevert, M. Rossle, N. Paust, D.I. Svergun, F.V. Stetten, R. Zengerle, D. Mark Lab on a Chip, 2016, 16, 1161. doi: 10.1039/C5LC01580D.
  10. S. Schewa, M.A. Schroer, T. Zickmantel, Y.-H. Song , C.E. Blanchet, A.Yu. Gruzinov, G. Katona, D.I. Svergun, M. Roessle Rev. Sci. Instrum., 2020, 91, 084101. doi: 10.1063/5.0004706.
  11. D. Garcia-Lojo, E. Modin, S. Gomez-Grana, M. Imperor-Clerc, A. Chuvilin, I. Pastoriza-Santos, J. Perez-Juste, D. Constantin, C. Hamon Adv. Funct. Mater., 2021, 31(27), 2101869. doi: 10.1002/adfm.202101869.
  12. N. Iranpour Anaraki, A. Sadeghpour, K. Iranshahi, C. Toncelli, U. Cendrowska, F. Stellacci, A. Dommann, P. Wick, A. Neels Nanoresearch, 2020, 13(10), 2847. doi: 10.1007/s12274-020-2940-4.
  13. T. Lange, S. Charton, T. Bizien, F. Testard, F. Malloggi Lab on a Chip, 2020, 20, 2990. doi: 10.1039/D0LC00454E.
  14. A.A. Guda, M.V. Kirichkov, V.V. Shapovalov, A.I. Muravlev, D.M. Pashkov, S.A. Guda, A.P. Bagliy, S.A. Soldatov, S.V. Chapek, A.V. Soldatov J. Phys. Chem. C., 2023, 127(2), 1097. doi: 10.1021/acs.jpcc.2c06625.
  15. D.S. Khvostichenko, E. Kondrashkina, S.L. Perry, A.S. Pawate, K. Brister ,P.J.A. Kenis Analyst, 2013, 138, 5384. doi: 10.1039/C3AN01174G.
  16. A. Ghazal, J.P. Lafleur, K. Mortensen, J.P. Kutter, L. Arleth, G.V. Jensen Lab on a Chip, 2016, 16, 4263. doi: 10.1039/C6LC00888G.
  17. B.F.B. Silva Phys. Chem. Chem. Phys., 2017, 19, 23690. DOI: 2017/cp/c7cp02736b.
  18. K. Khaliqi, A. Ghazal, I.D.M. Azmi, H. Amenitsch, K. Mortensen, S. Salentinig, A. Yaghmur Analyst, 2017, 142, 3118. DOI: 2017/an/c7an00860k.
  19. H.P. Martin, N.J. Brooks, J.M. Seddon, P.F. Luckham, N.J. Terrill, A.J. Kowalski, J.T. Cabral Soft Matter, 2016, 12, 1750. doi: 10.1039/C5SM02689J.
  20. Y. Zhang, Y. Dai, G. Tie, H. Hu App. Opt., 2016, 55(29), 8308. doi: 10.1364/AO.55.008308.
  21. A.P. Hammersley J. Appl. Crystallogr., 2016., 49(2), 646. doi: 10.1107/S1600576716000455.
  22. P.V. Konarev, V.V. Volkov, A.V. Sokolova, M.H.J. Koch, D.I. Svergun J. Appl. Crystallogr., 2003, 36, 1277. doi: 10.1107/S0021889803012779.
  23. A. Guinier Ann. Ph., 1939, 11(12), 161. doi: 10.1051/anphys/193911120161.
  24. A. Guinier, G. Fournet Small-Angle Scattering of X-rays, USA, NY, New York, Wiley: New York, 1955, 268 pp.
  25. D.I. Svergun J. Appl. Crystallogr., 1992, 25(4),495. doi: 10.1107/S0021889892001663.
  26. M.V. Kovalchuk, O.A. Alekseeva, A.E. Blagov, G.D. Ilyushin, K.B. Ilina, P.V. Konarev, V.A. Lomonov, Yu.V. Pisarevsky, G.S. Peters Crystallogr. Rep., 2019, 64(1), 6. doi: 10.1134/S1063774519010140.
  27. D.I. Svergun, C. Barberato, M.H.J. Koch J. Appl. Crystallogr., 1995, 28(6), 768. doi: 10.1107/S0021889895007047.
  28. A.M. Popov, A.S. Boikova, V.V. Volkov, Yu.A. D’yakova, K.B. Ilina, P.V. Konarev, M.A. Marchenkova, G.S. Peters, Yu.V. Pisarevskii, M.V. Koval’chuk Crystallogr. Rep., 2018, 64(5), 713. doi: 10.1134/S1063774518050231.
  29. M.A. Marchenkova, P.V. Konarev, A.S. Boikova, K.B. Ilina, Yu.V. Pisarevsky, M.V. Kovalchuk Crystallogr. Rep., 2021, 66, 751. doi: 10.1134/S1063774521050138.
  30. M.A. Marchenkova, S.V. Chapek, P.V. Konarev, K.B. Ilina, G.S. Peters, Yu.V. Pisarevsky, V.A. Shishkov, A.V. Soldatov, M.V. Kovalchuk Cryastals, 2023, 13, 938. doi: 10.3390/cryst13060938.
  31. A.E. Sukhanov, K.B. Ilina, P.V. Konarev, G.S. Peters, Yu.V. Pisarevsky, E.S. Smirnova, O.A. Alekseeva, M.V. Kovalchuk Crystals, 2023, 13(1),26. doi: 10.3390/cryst13010026.
  32. M.A. Marchenkova, P.V. Konarev, A.S. Boikova, K.B. Ilina, Yu.V. Pisarevsky, M.V. Kovalchuk Crystallogr. Rep., 2021, 66, 751. doi: 10.1134/S1063774521050138.

Қосымша файлдар

Қосымша файлдар
Әрекет
1. JATS XML

© Sukhanov A.E., Volkov V.V., Marchenkova M.A., Konarev P.V., Paul S.Y., Peters G.S., Pisarevsky Y.V., Chapek S.V., Shishkov V.A., Soldatov A.V., Kovalchuk M.V., 2024

Согласие на обработку персональных данных

 

Используя сайт https://journals.rcsi.science, я (далее – «Пользователь» или «Субъект персональных данных») даю согласие на обработку персональных данных на этом сайте (текст Согласия) и на обработку персональных данных с помощью сервиса «Яндекс.Метрика» (текст Согласия).