Reactions of  N -Allyl- and  N , N -Diallyltrifluoromethanesulfonamides with Carboxylic Acid Amides under Oxidizing Conditions

V. V. Astakhova; M. Yu. Moskalik; A. S. Ganin; B. A. Shainyan

doi:10.1134/S1070428018060052

Reactions of N-Allyl- and N,N-Diallyltrifluoromethanesulfonamides with Carboxylic Acid Amides under Oxidizing Conditions

作者: Astakhova V.V.¹, Moskalik M.Y.¹, Ganin A.S.¹, Shainyan B.A.¹
隶属关系:
1. Favorskii Irkutsk Institute of Chemistry, Siberian Branch
期: 卷 54, 编号 6 (2018)
页面: 855-860
栏目: Article
URL: https://bakhtiniada.ru/1070-4280/article/view/218047
DOI: https://doi.org/10.1134/S1070428018060052
ID: 218047

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Reactions of acetamide and benzamide with N-allyltrifluoromethanesulfonamide in the presence of t-BuOCl–NaI afforded exclusively 2,5-bis(chloromethyl)-1,4-bis(trifluoromethanesulfonyl)piperazine. Analogous reaction with N,N-diallyltrifluoromethanesulfonamide gave mixed halogenation product at only one C=C double bond of the substrate.