Composition and reactivity of aminolysis products of phenyl glycidyl ether with benzylamine

V. A. Pal’chikov; S. Yu. Mykolenko; A. N. Pugach; F. I. Zubkov

doi:10.1134/S1070428017050037

Composition and reactivity of aminolysis products of phenyl glycidyl ether with benzylamine

作者: Pal’chikov V.A.¹, Mykolenko S.Y.², Pugach A.N.², Zubkov F.I.³
隶属关系:
1. Oles’ Honchar Dnepropetrovsk National University
2. Dnepropetrovsk State Agrarian and Economic University
3. RUDN University
期: 卷 53, 编号 5 (2017)
页面: 656-662
栏目: Article
URL: https://bakhtiniada.ru/1070-4280/article/view/216172
DOI: https://doi.org/10.1134/S1070428017050037
ID: 216172

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Composition of aminolysis products of phenyl glycidyl ether with benzylamine in various conditions was studied. The ratio of 1-(benzylamino)-3-phenoxypropan-2-ol and 1,1'-(benzylazanediyl)bis(3-phenoxypropan-2-ol) does not considerably depend on the nature of the solvent and is basically determined by ratio of initial reagents. 2,6-Bis(phenoxymethyl)morpholine was obtained by dehydration of aminodiol in conditions of Mitsunobu reaction with subsequent reductive debenzylation.