Reaction of 3,4-dioxohexane-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine

P. P. Mukovoz; V. O. Koz’minykh; P. A. Slepukhin; I. N. Ganebnykh; O. S. El’tsov; A. V. Gorbunova; E. N. Koz’minykh

doi:10.1134/S1070428016050043

Reaction of 3,4-dioxohexane-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine

作者: Mukovoz P.P.¹, Koz’minykh V.O.², Slepukhin P.A.³^,4, Ganebnykh I.N.³^,4, El’tsov O.S.⁴, Gorbunova A.V.⁵, Koz’minykh E.N.²
隶属关系:
1. Moscow Technologic Institute
2. Perm State Humanitarian and Pedagogical University
3. Postovskii Institute of Organic Synthesis, Ural Branch
4. El’tsin Ural Federal University
5. Orenburg State University
期: 卷 52, 编号 5 (2016)
页面: 636-643
栏目: Article
URL: https://bakhtiniada.ru/1070-4280/article/view/214270
DOI: https://doi.org/10.1134/S1070428016050043
ID: 214270

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详细

Reaction was studied of 3,4-dihydroxyhexa-2,4-diene-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine that led to the formation of esters of (3E)-3-[2-(2,4-dinitrophenyl)-hydrazinylidene]-4-oxohexane-1,6-dioic and (3E,4E)-3,4-bis[2-(2,4-dinitrophenyl)hydrazinylidene]-hexane-1,6-dioic acids. The structural features of compounds synthesized were established from the data of IR and NMR spectra and X-ray diffraction (XRD) analysis.