Email this article One-Step Synthesis of Phosphorylated Vinylacethylene Derivatives
- Authors: Brel V.K.1
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Affiliations:
- A.N. Nesmeyanov Institute of Organoelement Compounds of the Russian Academy of Sciences
- Issue: Vol 89, No 11 (2019)
- Pages: 2212-2218
- Section: Article
- URL: https://bakhtiniada.ru/1070-3632/article/view/223153
- DOI: https://doi.org/10.1134/S1070363219110082
- ID: 223153
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Abstract
A one-step method for the preparation of 3-substituted 2-(diethylphosphoryl)but-1-en-3-ynes was developed based on the reaction of phosphorylated α-allene alcohols with methanesulfonic anhydride in the presence of triethylamine. The obtained vinylacetylene derivatives are of interest as promising precursors for the creation of organophosphorus heterocyclic compounds.
About the authors
V. K. Brel
A.N. Nesmeyanov Institute of Organoelement Compounds of the Russian Academy of Sciences
Author for correspondence.
Email: v_brel@mail.ru
Russian Federation, Moscow, 119991
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