1H NMR spectra and crystal structure of the nickel(II) complex with ethyl 5,5-dimethyl-2,4-dioxohexanoate aroylhydrazones


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Nickel(II) complexes NiLn ∙ NH3 (n = 1–5) with the products of condensation of ethyl 5,5-dimethyl-2,4-dioxohexanoate with aromatic acid hydrazides (H2L1–H2L5) were synthesized. The complexes were studied by elemental analysis and IR and 1H NMR spectroscopy. The structure of the complex NiL1 ∙ NH3 was determined by X-ray diffraction (CIF file CCDC no. 1057268).

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M. Tursunov

Bukhara State University

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Email: tursunovma@mail.ru
乌兹别克斯坦, Bukhara

K. Avezov

Bukhara State University

Email: tursunovma@mail.ru
乌兹别克斯坦, Bukhara

B. Umarov

Bukhara State University

Email: tursunovma@mail.ru
乌兹别克斯坦, Bukhara

N. Parpiev

Bukhara State University

Email: tursunovma@mail.ru
乌兹别克斯坦, Bukhara

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