电邮这篇文章 Mechanochemical synthesis of ni/hfc composite structures
- 作者: Grigoreva T.F1, Dudina D.V1,2, Vidyuk T.M1,3, Kovaleva S.A4, Ukhina A.V1, Devyatkina E.T1, Vosmerikov S.V1, Lyakhov N.Z1
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隶属关系:
- Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences
- Lavrentyev Institute of Hydrodynamics of the Siberian Branch of the Russian Academy of Sciences
- Khristianovich Institute of Theoretical and Applied Mechanics of the Siberian Branch of the Russian Academy of Sciences
- Joint Institute of Mechanical Engineering of the National Academy of Sciences of Belarus
- 期: 编号 3 (2025)
- 页面: 42-49
- 栏目: Articles
- URL: https://bakhtiniada.ru/0869-5733/article/view/315235
- DOI: https://doi.org/10.31857/S0869573325034249
- ID: 315235
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详细
The structural-phase evolution of the mechanochemical formation of Ni/HfC mechanocomposites containing 50 and 70 wt.% nickel was studied using X-ray diffraction analysis, scanning electron microscopy, and energy dispersive spectroscopy. It has been shown by X-ray diffraction analysis, that during mechanochemical synthesis in a ternary mixture of elemental powders Ni, Hf and C at a stoichiometric ratio of Hf and C, the formation of hafnium carbide occurred already after 40 s. For both compositions, the crystallite sizes of the nickel rapidly decrease upon mechanical activation for up to 4 min compared to the initial. Intensive formation of hafnium carbide is recorded during mechanical activation with duration of 4–8 minutes. With mechanical activation for 12 and 20 min, the processes of secondary structure formation lead to homogenization of the product and depletion of hafnium carbide in carbon to the composition HfС0.5.
作者简介
T. Grigoreva
Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences
Email: grig@solid.nsc.ru
D. Dudina
Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences; Lavrentyev Institute of Hydrodynamics of the Siberian Branch of the Russian Academy of Sciences
Email: grig@solid.nsc.ru
T. Vidyuk
Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences; Khristianovich Institute of Theoretical and Applied Mechanics of the Siberian Branch of the Russian Academy of Sciences
Email: grig@solid.nsc.ru
S. Kovaleva
Joint Institute of Mechanical Engineering of the National Academy of Sciences of Belarus
Email: grig@solid.nsc.ru
A. Ukhina
Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences
Email: grig@solid.nsc.ru
E. Devyatkina
Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences
Email: grig@solid.nsc.ru
S. Vosmerikov
Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences
Email: grig@solid.nsc.ru
N. Lyakhov
Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences
编辑信件的主要联系方式.
Email: grig@solid.nsc.ru
参考
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