Synthesis of MgFe 1.6 Ga 0.4 O 4  by Gel Combustion Using Glycine and Hexamethylenetetramine

M. N. Smirnova; M. A. Kop’eva; E. N. Beresnev; L. V. Goeva; N. P. Simonenko; G. E. Nikiforova; V. A. Ketsko

doi:10.1134/S0036023618040198

Synthesis of MgFe_1.6Ga_0.4O₄ by Gel Combustion Using Glycine and Hexamethylenetetramine

Authors: Smirnova M.N.¹, Kop’eva M.A.¹, Beresnev E.N.¹, Goeva L.V.¹, Simonenko N.P.¹, Nikiforova G.E.¹, Ketsko V.A.¹
Affiliations:
1. Kurnakov Institute of General and Inorganic Chemistry
Issue: Vol 63, No 4 (2018)
Pages: 439-443
Section: Synthesis and Properties of Inorganic Compounds
URL: https://bakhtiniada.ru/0036-0236/article/view/168574
DOI: https://doi.org/10.1134/S0036023618040198
ID: 168574

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Abstract

A powderlike material of composition MgFe_1.6Ga_0.4O₄ was synthesized by gel combustion using a glycine–hexamethylenetetramine mixture. The gel produced by the synthesis was studied by thermal analysis (TGA/DSC) and IR spectroscopy. This mixture was shown to be efficient for obtaining homogeneous nanosized MgFe_1.6Ga_0.4O₄. The morphology of the powders was characterized by scanning electron microscopy and X-ray powder diffraction analysis.