Effect of torsion conditions under high pressure on the structure and strengthening of the Zr–1% Nb alloy

Resumo

The effect of temperature and degree of deformation upon severe plastic deformation by torsion under a high pressure on the structure, phase composition, and microhardness of the industrial zirconium Zr–1% Nb alloy (E110) has been studied. The high-pressure torsion (HPT) (with N = 10 revolutions) of the Zr–1% Nb alloy at room temperature results in the formation of grain–subgrain nanosize structure with an average size of structural elements of 65 nm, increase in the microhardness by 2.3–2.8 times (to 358 MPa), and α-Zr → β-Zr and α-Zr → ω-Zr phase transformations. The increase in the HPT temperature to 200°C does not lead to a decrease in the microhardness of alloy owing to the increase in the fraction of ω-Zr phase, though the average size of structural elements increases to 125 nm. The increase in the temperature to 400°C during HPT with N = 10 revolutions leads to the grain growth in the α-Zr grain structure (~90%) to 160 nm and a decrease in the microhardness to 253–276 HV.