


Vol 117, No 4 (2016)
- Year: 2016
- Articles: 11
- URL: https://bakhtiniada.ru/0031-918X/issue/view/10165
Article
Physical metallurgy: Scientific school of the Academician V.M. Schastlivtsev
Abstract
This paper is to honor Academician Vadim Mikhailovich Schastlivtsev, a prominent scientist in the field of metal physics and materials science. The article comprises an analysis of the topical issues of the physical metallurgy of the early 21st century and of the contribution of V.M. Schastlivtsev and of his school to the science of phase and structural transformations in steels. In 2015, Vadim Mikhailovich celebrates his 80th birthday, and this paper is timed to this honorable date. The list of his main publications is given in it.



Electrical and Magnetic Properties
Asymmetric pinning of vortex domain walls in magnetic films in regions with lowered saturation magnetization
Abstract
The asymmetric pinning of vortex domain walls in a region with a lowered saturation magnetization has been investigated in ferromagnetic films with the in-plane anisotropy. Numerical micromagnetic simulation within the two-dimensional model of the magnetization distribution has been used. The wall structure and the depinning fields in different directions have been investigated depending on the dimensions of the region with lowered saturation magnetization and the film thickness. The physical factors that determine the obtained regularities have been established.



Structure, Phase Transformations, and Diffusion
Effect of temperature of HPT deformation and the initial orientation on the structural evolution in single-crystal niobium
Abstract
The structural evolution and hardness of sing-crystal niobium with various initial orientations are investigated after its deformation in Bridgman anvils at room (290 K) and cryogenic (80 K) temperatures. It is shown that no twinning occurs upon cryogenic deformation; thin prolonged bands dividing the matrix into weakly misoriented regions are formed. The uniform-in-size structure of a nanoscale level (dav = 40 nm) is formed during cryogenic deformation after the maximum achieved true strain. The average microcrystallite size observed after room-temperature deformation is 120 nm.



Defects in a lattice of pure nickel subjected to fast-neutron irradiation followed by annealings: Neutron-diffraction examination
Abstract
Nickel specimens subjected to fast-neutron irradiation followed by annealings have been examined using neutron and X-ray diffraction. The type of structural defects, which result from the fast-neutron irradiation of nickel crystals, has been first identified using neutron diffraction and the experimental dependence of the lattice parameter on the concentration of interstitial defects has been determined. It is shown that the changes in the lattice parameters due to both irradiation and annealings are primary related to the variations in the concentration of interstitial atoms in the lattice.



Dislocation structure of martensitic transformation in carbon steel
Abstract
The developed method of diffraction analysis has shown that the martensitic transformation in iron crystals with the interstitial carbon atoms produces the highest natural density of dislocations in metals. The transformation occurs via microscopic shears, which collectively rearrange the lattice. This process becomes more evident due to the high concentration of fine dislocation loops, which has initially been identified in cubic and then in tetragonal martensite crystals.



Strength and Plasticity
Constitutive relations for determining the critical conditions for dynamic recrystallization behavior
Abstract
A series mathematical model has been developed for the prediction of flow stress and microstructure evolution during the hot deformation of metals such as copper or austenitic steels with low stacking fault energies, involving features of both diffusional flow and dislocation motion. As the strain rate increases, multiple peaks on the stress-strain curve decrease. At a high strain rate, the stress rises to a single peak, while dynamic recrystallization causes an oscillatory behavior. At a low strain rate (when there is sufficient time for the recrystallizing grains to grow before they become saturated with high dislocation density with an increase in strain rate), the difference in stored stress between recrystallizing and old grains diminishes, resulting in reduced driving force for grain growth and rendering smaller grains in the alloy. The final average grain size at the steady stage (large strain) increases with a decrease in the strain rate. During large strain deformation, grain size reduction accompanying dislocation creep might be balanced by the grain growth at the border delimiting the ranges of realization (field boundary) of the dislocation-creep and diffusion-creep mechanisms.



Effect of torsion conditions under high pressure on the structure and strengthening of the Zr–1% Nb alloy
Abstract
The effect of temperature and degree of deformation upon severe plastic deformation by torsion under a high pressure on the structure, phase composition, and microhardness of the industrial zirconium Zr–1% Nb alloy (E110) has been studied. The high-pressure torsion (HPT) (with N = 10 revolutions) of the Zr–1% Nb alloy at room temperature results in the formation of grain–subgrain nanosize structure with an average size of structural elements of 65 nm, increase in the microhardness by 2.3–2.8 times (to 358 MPa), and α-Zr → β-Zr and α-Zr → ω-Zr phase transformations. The increase in the HPT temperature to 200°C does not lead to a decrease in the microhardness of alloy owing to the increase in the fraction of ω-Zr phase, though the average size of structural elements increases to 125 nm. The increase in the temperature to 400°C during HPT with N = 10 revolutions leads to the grain growth in the α-Zr grain structure (~90%) to 160 nm and a decrease in the microhardness to 253–276 HV.



Mechanical characteristics and microstructure of weld joint of high-temperature martensitic steel containing 9% Cr
Abstract
The structure and mechanical characteristics of a weld joint of 10Kh9K3V2MFBR steel (0.097 C, 0.17.Si, 0.54 Mn, 8.75 Cr, 0.21 Ni, 0.51 Mo, 0.07 Nb, 0.23 V, 0.004 N, 0.003 B, 1.6 W, 0.15 Cu, and Fe for balance, wt %) have been studied; the joint was produced by hand welding in an argon atmosphere using 03Kh20N45M7G6B welding wire (0.3 C, 20 Cr, 45 Ni, 7 Mo, 6 Mn, and 1 Nb, wt %). The weld joint is divided into the zone of the base metal, a thermal effect zone, which consists of zones that contain fine and coarse original austenitic grains, and the zone of seam metal. It has been shown that the weld joint of 10Kh9K3V2MFBR steel possesses high strength characteristics at the room temperature under static loading and a satisfactorily impact toughness, which has the minimum value of 30 J/cm2 in the zone of the seam metal and does not depend on the temperature. With a decrease in the temperature from the room temperature to 253 K, a ductile–brittle transition occurs in the thermal effect zone. Creep tests carried out at the temperature of 923 K have shown that the long-term strength of the weld seam is lower than that of the base material in the entire stress range being tested. At stresses of 140 MPa or higher, the acceleration of creep in the weld seam is observed, while at low stresses of about 120 MPa, the rates of creep in the weld seam and in the base metal remain similar until the transition to the stage of accelerated fracture occurs. The difference in the values of the long-term strength is due to premature fracture, which occurs in the thermal effect zone with the finegrained structure.



Mechanical behavior and brittle–ductile transition of high-chromium martensitic steel
Abstract
The article presents data on the static tensile tests and dynamic impact-toughness tests of a highchromium martensitic 10Kh9V1M1FBR steel (0.12 wt % C, 9.8 wt % Cr, 0.93 wt % W, 1.01 wt % Mo, 0.2 wt % V, 0.05 wt % Nb, 0.05 wt % N, 0.003 wt % B, 0.36 wt % Mn, 0.2 wt % Ni, 0.06 wt % Si, 0.01 wt % P, 0.008 wt % S, 0.02 wt % Cu, 0.1 wt % Co, 0.015 wt % Al, and the remainder is Fe) in the temperature range from 20 to–196°C. In the case of static loading, a reduction in the temperature leads to an increase in the strength characteristics; upon a drop in the temperature from 20 to–100°C, the plasticity also increases. This is connected with the fact that the ductile fracture remains the basic mechanism down to cryogenic temperatures. The brittle–ductile transition related to the transition from ductile intragranular fracture to quasibrittle one is observed at–45°C. The steel exhibits high impact toughness to the temperature of–60°C (KCV–60 = 95 J/cm2), at which the fraction of the ductile component in fracture is equal to 20%. At 80°C, the impact toughness decreases down to critical values (30 J/cm2), which correlates with the decrease in the fraction of the ductile component on the fracture surface down to 1%. The further decrease in the impact toughness down to 10 J/cm2 at–196°C is related to the transition from intragranular to intergranular brittle fracture.



Migration and accumulation at dislocations of transmutation helium in austenitic steels upon neutron irradiation
Abstract
The model of the migration and accumulation at dislocations of transmutation helium and the formation of helium–vacancy pore nuclei in austenitic steels upon neutron irradiation has been proposed. As illustrations of its application, the dependences of the characteristics of pore nuclei on the temperature of neutron irradiation have been calculated. The results of the calculations have been compared with the experimental data in the literature on measuring the characteristics of radiation-induced porosity that arises upon the irradiation of shells of fuel elements of a 16Cr–19Ni–2Mo–2Mn–Si–Ti–Nb–V–B steel in a fast BN600 neutron reactor at different temperatures.



Separations in steels subjected to controlled rolling, followed by accelerated cooling
Abstract
Zones on the fracture surfaces of Charpy specimens and profiles of the fractures of these specimens are examined using impact-bending tests carried out in the temperature range of +20 to–90°C and fractography. The specimens were cut out of hot-rolled plates produced from 05G2B super-low-carbon steels that contained Ti, Nb, V, and Cu microadditives using controlled rolling, followed by accelerated cooling. A detailed analysis of separations, including a study of the morphology, number, area of separations, and the surrounding stress-relaxation zones, and the structure of the walls, has allowed us to identify the mechanisms of the origination and growth of the separations. It has been found that the correlated changes in the length, width, and depth of the separations are accompanied by the formation and expansion of the stress-relaxation zones around the separations. The rate of expansion of the area of these zones is higher than that of the area of the separations, which favors the macroplastic fracture of the specimens.


