Email this article Structural Characterization of 11-Ethyl-6,11-Dihydro-5H-Dibenzo[b,e]Azepine
- Authors: Delgado G.E.1, Osal E.1, Mora A.J.1, González T.2, Palma A.3, Bahsas A.4
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Affiliations:
- Laboratorio de Cristalografía, Departamento de Química, Facultad de Ciencias
- Centro de Química
- Laboratorio de Síntesis Orgánica, Escuela de Química
- Laboratorio de Resonancia Magnética Nuclear, Departamento de Química
- Issue: Vol 59, No 5 (2018)
- Pages: 1210-1214
- Section: Article
- URL: https://bakhtiniada.ru/0022-4766/article/view/162004
- DOI: https://doi.org/10.1134/S0022476618050281
- ID: 162004
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Abstract
The title compound C16H17N, a potential pharmaceutical agent, crystallizes in the monoclinic P21/n space group with unit cell parameters a = 9.911(7) Å, b = 5.542(3) Å, c = 23.245(16) Å, β = 96.25(2)°. The dibenzazepine ring adopts a twist-boat conformation. The crystal packing is entirely dominated by cohesive weak N–H⋯Cg(π) and Cg(π)⋯Cg(π) interactions among the neighboring molecules producing an efficient packing with 66.4% of the occupied space.
About the authors
G. E. Delgado
Laboratorio de Cristalografía, Departamento de Química, Facultad de Ciencias
Author for correspondence.
Email: gerzon@ula.ve
Venezuela, Bolivarian Republic of, Mérida
E. Osal
Laboratorio de Cristalografía, Departamento de Química, Facultad de Ciencias
Email: gerzon@ula.ve
Venezuela, Bolivarian Republic of, Mérida
A. J. Mora
Laboratorio de Cristalografía, Departamento de Química, Facultad de Ciencias
Email: gerzon@ula.ve
Venezuela, Bolivarian Republic of, Mérida
T. González
Centro de Química
Email: gerzon@ula.ve
Venezuela, Bolivarian Republic of, Caracas
A. Palma
Laboratorio de Síntesis Orgánica, Escuela de Química
Email: gerzon@ula.ve
Colombia, Bucaramanga
A. Bahsas
Laboratorio de Resonancia Magnética Nuclear, Departamento de Química
Email: gerzon@ula.ve
Venezuela, Bolivarian Republic of, Mérida
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