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Том 61, № 4 (2018)

Application of Computers in Experiments

A Data Buffering and Transmission System: A Study of the Performance of a Disk Subsystem

Bezrukov I., Salnikov A., Yakovlev V., Vylegzhanin A.

Аннотация

A method for evaluation of the performance of the disk subsystem of a data buffering and transmission system and results of experimental studies of the performance of the disk subsystem according to the developed method are presented. A conclusion is drawn on the reasonability of the use of hard-disk drives that provide the required read/write rates with a sufficiently high level of reliability in prospective development of the modern high-capacity NearLine SAS (NL-SAS).

Instruments and Experimental Techniques. 2018;61(4):467-472
pages 467-472 views

A Data Stream Converter for a Radio Telescope with a Wideband-Signal Digital Recording System

Grenkov S., Kol’tsov N.

Аннотация

A data-stream converter makes it possible to connect a radio telescope with wideband (512 MHz) signal-recording channels to active very-long-baseline interferometers using multichannel recording systems for narrowband (16 or 8 MHz) signals. A digital converter based on a field programmed gate array (FPGA) selects and formats up to 16 narrowband signals.

Instruments and Experimental Techniques. 2018;61(4):473-481
pages 473-481 views

The Automation of a CVD-Reactor for the Synthesis of Vertically Oriented Carbon Nanotube Arrays

Gusel’nikov A., Safronov A., Kurenya A., Arkhipov V., Bolgarin S., Ivanov A., Kvashnin A., Okotrub A.

Аннотация

The functional diagram and the automation system of a CVD-reactor for the synthesis of vertically oriented carbon nanotube arrays on silicon substrates are described. The system is intended predominantly for recording the physical parameters of the CVD-reactor in real time, generating the instructions for the operator on the selected synthesis-process flow, on-screen display of the selected parameters, and management of the automatic protection of the reactor units and assemblies against contingencies or unspecified actions of the operator. The structure of the system for data acquisition, visualization of synthesis variables, and the CVD process control that allows the synthesis of vertically oriented carbon nanotube arrays is presented.

Instruments and Experimental Techniques. 2018;61(4):482-485
pages 482-485 views

Electronics and Radio Engineering

An Acoustic Time-Delay Meter

Shkelev E., Shirkaev A.

Аннотация

An FPGA-based acoustic time-delay meter with the post-detection correlation processing of pseudo-noise signals is proposed. The measurement method is based on the real-time computation of the mutual correlation function between the reference signal that follows the modulation law and the received signal. The experimental results obtained using a prototype of the developed system are presented. The results validated the viability of the developed software and hardware solutions as applied to acoustic-, radio-, and hydroacoustic-location systems.

Instruments and Experimental Techniques. 2018;61(4):486-490
pages 486-490 views

Generation of High-Voltage Pulses with a Picosecond Front in a Cascade Kivotron Connection

Bokhan P., Gugin P., Zakrevsky D., Lavrukhin M.

Аннотация

The possibility of the operation of high-current high-voltage switches based on “open” discharge with the generation of counter-propagating electron beams, that is, kivotrons, in a two-stage pulse compression scheme is demonstrated experimentally. The total degree of the initial-pulse compression, which exceeded 600 at a minimum measured front duration of a generated pulse of at most 100 ps, was achieved at a voltage of up to 18 kV and a pulse-repetition rate of 1 kHz.

Instruments and Experimental Techniques. 2018;61(4):491-495
pages 491-495 views

Investigation of Silicon Diodes in the Mode of Switching by an Impact-Ionization Wave

Korotkov S., Aristov Y., Voronkov V., Korotkov D.

Аннотация

The results of investigations of silicon diodes in the mode of switching by nanosecond pulses, which initiate an impact-ionization wave, are presented. It is shown that the switching process is significantly influenced by dislocations that are formed in the surface layers of diode structures during their manufacture.

Instruments and Experimental Techniques. 2018;61(4):496-500
pages 496-500 views

The Coaxial Shunt for Measurement of Current Pulses of Artificial Lightning with the Amplitude up to ±220 kA

Baranov M., Kniaziev V., Rudakov S.

Аннотация

The improved construction of the coaxial shunt SC-300M intended for measurement of decaying sine and aperiodic pulses of artificial lightning current with amplitudes up to ±220 kA is described. The results of tests of the instrument shunt in the high-current discharging circuit of power high-voltage generator of lightning current (g.l.c.) under pulsed A-component with the first amplitude -198 kA corresponding to time ≈35 µs and an action integral of the simulated pulse of current of lightning discharge equal to ≈2.38 × 106 J/Ω are presented. The quantity of electricity under single action on the shunt by a current pulse of artificial lightning with logarithmic decrement of oscillations ≈2.06 that passed through the current-carrying elements of its construction was ≈-9.9 C. It was shown that, simultaneously with registration of pulsed A-component of lightning current, the shunt, owing to using of a matching voltage divider at the end of its cable communication line, allows also to measure normalized amplitude-time parameters of aperiodic shortened long-term C*-component of artificial lightning current (-568 A; ≈5 ms;τC* ≈18 ms; -16 C) that was being formed in the discharging circuit of the generator.

Instruments and Experimental Techniques. 2018;61(4):501-505
pages 501-505 views

A Programmable Pulse Sequence Generator for High Temperature Low-Field NMR Apparatus

Zhang J., Fan Y., Cheng J., Wu L., Xu Y.

Аннотация

The stable operation of pulse sequence generators at high temperatures (200°C) has been an important issue for some time in the application of nuclear magnetic resonance (NMR) apparatus for oil exploration. The application of system-in-package (SiP) technology was used to improve the temperature-resist grade of the hardware platform. A pulse sequence generator that meets the requirements of accurate phase and adjustable frequency during NMR apparatus in high temperature environments was designed and implemented. At ambient temperatures of up to 200°C, experimental results show that the delay times of the rising and falling edges of the pulse are 3.2 and 3.35 ns. respectively. The eye diagram Q factor of the critical path is not less than 15, and the Bit Error Rate (BER) is not more than 10–50. The experimental results show that a pulse sequence generator can meet the requirements of high temperature NMR apparatus, and can also provide a template for the design of an NMR pulse sequence generator for special fields of application, such as deep sea surveys and aviation.

Instruments and Experimental Techniques. 2018;61(4):506-515
pages 506-515 views

Frequency Tuning of a Magnetron of the 3-mm Wavelength Range Using an Additional Output

Skripkin N., Morugin S.

Аннотация

The frequency tuning of a magnetron that operates on a spatial harmonic of the π/2–1 oscillation type was investigated. The mechanisms that limit the frequency-tuning range upon a change in the electric length of an additional (second) energy output were clarified and the possibilities of creating preferable conditions for exciting an operating oscillation mode by changing the external quality factor via rotation of the electromagnetic-field structure were determined. Based on calculations, experimental prototypes of magnetrons were manufactured and investigated. Long-term stable oscillations with a power of up to 11.5 kW were achieved. The tuning range using the second output is 300 MHz with a decrease in the output power down to 68% relative to the maximum power. The tuning range is up to 600 MHz at a power level of ~30% of the maximum and a reduced anode voltage.

Instruments and Experimental Techniques. 2018;61(4):516-520
pages 516-520 views

Coherent Summation of Wave Fields of Nanosecond Gunn Oscillators with Initial Phases Fixed by the Leading Edges of Electric Pulses from Synchronized Modulators

Barmin V., Klimov A., Kovalchuk O., Konev V.

Аннотация

Coherent summation was performed for the wave fields of pairs of X-band nanosecond Gunn oscillators based on 3A762 diodes. Each oscillator was excited by its own modulator. The initial phase of the microwave pulse of each oscillator was fixed by the leading edge of the electrical pulse from the respective modulator. The modulators were triggered by a common sync pulse. The total microwave-radiation patterns of antenna pairs connected to the Gunn oscillators were in good agreement with the total radiation patterns of these antennas excited in phase by a standard oscillator.

Instruments and Experimental Techniques. 2018;61(4):521-524
pages 521-524 views

General Experimental Techniques

A Method for Increasing the Sensitivity of Mass-Spectrometric Measurements

Anufriev G.

Аннотация

A method for increasing the sensitivity of mass-spectrometric measurements in the analysis of small amounts of gases, which are insufficient for organizing a stationary flow through an ion source, is considered. Measurements are carried out upon a single injection of a portion of a gas. The use of this method for increasing the sensitivity in isotope helium analyses on MI9303 magnetic-resonance mass spectrometers allowed the sensitivity of the spectrometer to be increased to ~105 atoms in a sample, i.e., it allowed measurements for a helium volume in a sample of up to ~10−14 cm3. The experience of carrying out isotope analyses in samples of inert gases of various origins using different methods for evacuating chambers of mass analyzers was generalized.

Instruments and Experimental Techniques. 2018;61(4):525-529
pages 525-529 views

Measurements of the Ion-Beam Current Distribution over a Target Surface under a High Bias Potential

Mamedov N., Prokhorovich D., Yurkov D., Kanshin I., Solodovnikov A., Kolodko D., Sorokin I.

Аннотация

A technique for direct measurements of the current distribution over the surface of a target that is at a negative bias potential relative to the ground was developed and tested. Measurements were performed using a six-channel meter that transmitted the measured data through a wireless Bluetooth acquisition system. The trace of an ion flow on the target surface was visualized by the method of luminous beams. Examples of the measured current distributions on a target surface depending on the geometric and physical parameters of the ion-optical system of a Penning plasma source are presented.

Instruments and Experimental Techniques. 2018;61(4):530-537
pages 530-537 views

An Ion Source for a Plasma-Optic Mass Separator

Bardakov V., Kazantsev A., Strokin N., Stupin A.

Аннотация

A device for forming an ion beam in a plasma-optic mass separator was developed on the basis of a two-chamber plasma accelerator—thruster—with anodic layers (TAL). The anode of the second chamber in the TAL is replaced with an azimuthator of the mass separator. Functionally, the azimuthator plays the role of the cathode for both the first and second accelerator chambers. This becomes possible after a potential that is negative with respect to the TAL anode is applied to the azimuthator–cathode. The ion source has been tested as a part of the POMS-E-3 mass separator. The ion density at the output of the source is 2–4 times higher than the density at the output of the “classical” two-chamber TAL.

Instruments and Experimental Techniques. 2018;61(4):538-542
pages 538-542 views

Probe Diagnostics of a Rotating Plasma

Gorshunov N., Potanin E.

Аннотация

A technique for making probe measurements of the parameters of a plasma rotating in crossed radial electric and axial magnetic fields is described. Unlike the commonly used method, the processing of readings of the Langmuir triple probe was carried out using the results of measurements based on a Mach plasma probe. When using a magnetic field produced in a solenoid without end-to-end magnetic plugs, a positive potential with respect to the grounded anode and outer metal tube is observed in the plasma that arrives from the electric discharge source with the thermoemission cathode and the annular anode. It is shown that the speed of azimuthal electron drift in the crossed-fields system under investigation is much higher than the ion rotation speed.

Instruments and Experimental Techniques. 2018;61(4):543-547
pages 543-547 views

Automation of a Research Facility for Atomic Vapor Laser Isotope Separation

Panchenko V., Firsov V., Tsvetkov G., D’yachkov A., Gorkunov A., Labozin A., Mironov S.

Аннотация

The problems of introducing automation into experimental studies required for the development of an atomic vapor laser isotope separation method are considered. The investigations are carried out at a facility consisting of a vacuum module and a set of wavelength-tunable dye lasers pumped with copper vapor lasers. The vacuum module contains an atomic beam source, a quadrupole mass spectrometer, and a luminescence detection system. The approaches used to stabilize the laser wavelength and to scan the laser wavelength with the simultaneous recording of the mass-spectrometer and luminescence signals in strong high-frequency electromagnetic fields accompanying the operation of copper vapor lasers are also considered. Examples of experimental results are presented.

Instruments and Experimental Techniques. 2018;61(4):548-555
pages 548-555 views

A Fluorimeter on the Basis of a Femtosecond Cr+4: Forsterite Laser

Shandarov Y., Kryukov I., Ivanov D., Ivanov A., Petrov N., Alfimov M.

Аннотация

An apparatus for measuring luminescence lifetimes using the femtosecond up-conversion method is presented. A laser system based on a chromium–forsterite crystal with a lasing wavelength of 1250 nm is used to generate ultrashort pulses. Luminescence is excited in a sample by optical harmonics that are generated in nonlinear optical crystals. The width of the instrument function of the system is 200 fs. Methods for optimizing the signal-to-noise ratio in measurements are discussed. The results of measurements of the fluorescence- decay dynamics and the anisotropy of aqueous solutions of an inclusion complex of the 4-DASPI styrene dye in cucurbit[6]uril on short (5 ps) and long (500 ps) time scales are presented.

Instruments and Experimental Techniques. 2018;61(4):556-561
pages 556-561 views

A Spectral–Thermal Bench with a Special Fiber-Optic Probe–Objective for Measuring Diffuse-Reflection Spectra

Kuptsov A., Arutyunov I., Zhmaeva E., Kulik A.

Аннотация

The results of tests of a new fiber-optic probe–objective for measuring both IR diffuse-reflection spectra and other types of spectra of solids at various temperatures are presented. In comparison with the conventional devices, the new scheme for measuring diffuse-reflection spectra has such advantages as the minimum distortion of spectra by the specular and Fresnel diffuse components of the reflection from surface irregularities and the linearity of the concentration dependences. The use of a fiber-optic probe–objective provides the ability for the simultaneous analysis of the solid phase and outgoing gases with increasing temperature and calibration of the spectral methods using the thermogravimetric-analysis data. An example of monitoring the process of drying catalysts in laboratory studies when analyzing composite and other materials is used to consider the prospects for using the probe–objective.

Instruments and Experimental Techniques. 2018;61(4):562-571
pages 562-571 views

Physical Instruments for Ecology, Medicine, and Biology

Calibration of the Spectra of Astronomical Objects

Panchuk V., Yakopov G., Klochkova V., Yushkin M.

Аннотация

The types of astronomical-spectrum calibrations in the wavelengths used in spectroscopy of stars at the 6-m BTA optical telescope are listed. A device has been developed for simultaneous recording of a star spectrum and a reference emission spectrum.

Instruments and Experimental Techniques. 2018;61(4):572-576
pages 572-576 views

A Complex for Carrying Out Radar Observations of Near-Earth Objects

Marshalov D., Bondarenko Y., Medvedev Y., Vavilov D., Zotov M., Mikhailov A.

Аннотация

The Institute of Applied Astronomy of the Russian Academy of Sciences and the Goldstone Deep Space Communications Complex regularly conduct intercontinental radar observations of near-Earth objects using a 70-m DSS-14 antenna as a transmitter and the 32-m RT-32 radio telescopes of the Quasar VLBI network as receivers. To carry out the observations, the existing complex for reception, conversion, and recording of signals from the RT-32 radio telescopes has been adapted and special software for scheduling observations and processing echo signals has been developed. Since 2015, echoes from the 2011 UW158, 2003 TL4, 2003 YT1, 2003 BD44, and 2014 JO25 asteroids have been recorded. The power spectra of the echoes from these asteroids have been obtained and analyzed.

Instruments and Experimental Techniques. 2018;61(4):577-582
pages 577-582 views

Reducing the Energy Consumption of a Laser Photo-Acoustic SF6 Gas Analyzer

Sherstov I., Vasiliev V., Karapuzikov A., Zenov K., Pustovalova R.

Аннотация

Experimental studies of the operating modes of a laser photo-acoustic SF6 gas analyzer that were aimed at reducing its energy consumption were carried out. It was shown in the experiments that an average power of CO2 laser radiation of at least 100 mW is required for the assured detection of low SF6 concentrations (less than 100 ppb). To reduce the energy consumption of the gas analyzer, it is proposed to decrease the repetition frequency of CO2 laser pulses by several times and operate on subharmonics of the resonance frequency of the photo-acoustic detector. The experimental results made it possible to reduce the energy consumption of the gas analyzer to ~15 V A and use a Li-ion battery from a laptop to power it. The duration of the continuous operation of the gas analyzer on one battery charge was at least 6 h.

Instruments and Experimental Techniques. 2018;61(4):583-589
pages 583-589 views

A Radio-Frequency Neck Quadrature Coil for Magnetic-Resonance Imaging

Bayazitov A., Chumarov P., Fattakhov Y.

Аннотация

The design features of the radio-frequency Neck receiving coil for low-field magnetic-resonance tomographs are described. The results of the study of the influence of the reflective contour on the receiving system are given for the purpose of improving the performance of the sensor. The results of comparison of patient images that were obtained using two different sensors are presented.

Instruments and Experimental Techniques. 2018;61(4):590-595
pages 590-595 views

Laboratory Techniques

Piezoceramic Gauges for Measuring Rapidly Changing and Oscillatory Pressures

Golub V., Zhilin Y., Marchuk N.

Аннотация

Designs of piezoelectric pressure gauges based on PZT-19 ceramics and equipment for testing and calibration of piezoelectric gauges are described. Tests of the developed piezoelectric transducers in a shock tube showed that their characteristics are stable in time, the sensitivity ranges from 5 to 50 mV/bar, the operating pressure range is up to 100 bar, and the frequency range with a high-resistivity matching amplifier is 10–5 × 105 Hz. The level of errors in measurements of pulse and oscillatory pressures is estimated as 5%.

Instruments and Experimental Techniques. 2018;61(4):596-603
pages 596-603 views

A Laboratory CVD Reactor for the Synthesis of Vertically Oriented Carbon Nanotube Arrays

Gusel’nikov A., Safronov A., Kurenya A., Arkhipov V., Bolgarin S., Ivanov A., Kvashnin A., Okotrub A.

Аннотация

The functional structure and the design of a CVD reactor for the synthesis of vertically oriented carbon nanotube (VOCNT) arrays on silicon substrates are described. To synthesize VOCNTs, various organic compounds, viz., toluene, cyclohexane, and acetonitrile, and their mixtures in the liquid state were tested under normal conditions.

Instruments and Experimental Techniques. 2018;61(4):604-609
pages 604-609 views

A Miniature Layered SAW Contact Stress Sensor for Operation in Cramped Metallic Slits

Li H., Ding J., Wei S., Chu B., Guan L., Du L., Liu G., He J.

Аннотация

Based on passive and wireless surface acoustic wave (SAW) sensing technology, a sensor terminal was designed to measure the contact stress in a cramped metallic slit with less than 0.5 mm in width. A layered structure of force-sensitive element with 0.5 mm in total thickness was put forward to package SAW resonator. Thin films with elasticity and flexibility were adopted to transfer load effectively between rigid surfaces. A flexible transmission line with double-stub structure and a patch microstrip antenna were used to realize the wireless interrogation to the sensor. The force-sensitive element model was built and simulated with FEA software (COMSOL Multiphysics). The sensor prototype exhibited significant linear and repeatable frequency shifts for the loads in the range of 0–4 MPa. The linearity error was ±3% of full-scale output (FSO), and the accuracy was ±1.25% FSO. The usage of elastic films in force-sensitive element caused hysteresis in output, but the hysteresis error was controlled in an acceptable range of ±3.8% FSO.

Instruments and Experimental Techniques. 2018;61(4):610-617
pages 610-617 views

Detection of Residual Oil Film on Polished KDP Crystal by Atomic Force Microscope

Guan L., Ding J., Zhang Y., Li H., Wang C., Wang W., Du L., He J.

Аннотация

In this paper, the bimodal amplitude-and frequency modulation method of atomic force microscopy (AFM) is applied to investigate the residual oil film on KDP crystal surface after polishing and surface cleaning. The thickness map of residual oil film is obtained based on the relationship between the cantilever resonant frequency shift and the surface stiffness. The thickness maps measured by AFM and spectroscopic imaging ellipsometry methods are compared, and the results obtained by two methods are consistent. The measurement scheme extends the application of AFM technology to characterize the residual oil on the KDP surface quality quantitatively after polishing and surface cleaning.

Instruments and Experimental Techniques. 2018;61(4):618-625
pages 618-625 views

An Experimental Setup for Investigation of Cryogenic Helium Plasma and Dusty Plasma Structures within a Wide Temperature Range

Boltnev R., Vasiliev M., Petrov O.

Аннотация

A new experimental setup for studying various phenomena in both cryogenic helium plasma and dusty plasma structures in a low-pressure gas discharge within the temperature range of 1.6–300 K is described. The setup is equipped with a modern data-acquisition system and high-speed video cameras to observe processes in dusty plasma structures. For the first time, dusty plasma structures were observed and studied at temperatures below 4 К.

Instruments and Experimental Techniques. 2018;61(4):626-629
pages 626-629 views