A Laboratory Apparatus for Spark Plasma Sintering of Ceramic and Composite Materials
- Autores: Asvarov A.S.1,2, Muslimov A.E.1, Akhmedov A.K.2, Abduev A.K.2, Kanevsky V.M.1
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Afiliações:
- Shubnikov Institute of Crystallography, Russian Academy of Sciences, Federal Research Center Crystallography and Photonics, Russian Academy of Sciences
- Amirkhanov Institute of Physics, Dagestan Scientific Center, Russian Academy of Sciences
- Edição: Volume 62, Nº 5 (2019)
- Páginas: 726-730
- Seção: Laboratory Techniques
- URL: https://bakhtiniada.ru/0020-4412/article/view/160935
- DOI: https://doi.org/10.1134/S0020441219050038
- ID: 160935
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Resumo
The design of a laboratory apparatus for spark plasma sintering of powder compositions of different compositions and purposes is described. The main active factors of the spark plasma sintering process, the nature and degree of their influence on the mechanism of consolidation of particles of powder mixtures, as well as the structure and properties of the synthesized ceramics are determined. The data on the synthesis of 25.4 mm ceramic disks of samarium monosulfide powder are given. It is shown that the optimization of the synthesis regimes allows one to obtain a compacted material with a density close to the theoretical one and a phase composition identical to the composition of the initial powder mixture.
Sobre autores
A. Asvarov
Shubnikov Institute of Crystallography, Russian Academy of Sciences,Federal Research Center Crystallography and Photonics, Russian Academy of Sciences; Amirkhanov Institute of Physics, Dagestan Scientific Center, Russian Academy of Sciences
Autor responsável pela correspondência
Email: cht-if-ran@mail.ru
Rússia, Moscow, 119333; Makhachkala, 367015
A. Muslimov
Shubnikov Institute of Crystallography, Russian Academy of Sciences,Federal Research Center Crystallography and Photonics, Russian Academy of Sciences
Email: cht-if-ran@mail.ru
Rússia, Moscow, 119333
A. Akhmedov
Amirkhanov Institute of Physics, Dagestan Scientific Center, Russian Academy of Sciences
Email: cht-if-ran@mail.ru
Rússia, Makhachkala, 367015
A. Abduev
Amirkhanov Institute of Physics, Dagestan Scientific Center, Russian Academy of Sciences
Email: cht-if-ran@mail.ru
Rússia, Makhachkala, 367015
V. Kanevsky
Shubnikov Institute of Crystallography, Russian Academy of Sciences,Federal Research Center Crystallography and Photonics, Russian Academy of Sciences
Email: cht-if-ran@mail.ru
Rússia, Moscow, 119333
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