Plasmachemical synthesis and basic properties of CoFe2O4 magnetic nanoparticles

Resumo

Cobalt-ferrite (CoFe₂O₄) nanoparticles (CFNPs) are obtained using direct plasmachemical synthesis in the plasma of a low-pressure arc discharge. The formation of the CFNPs with an average size of 9 nm and a narrow granulometric composition is established employing the methods of X-ray structure analysis and transmission microscopy. The CFNP behavior upon high-temperature annealing is analyzed. The CFNP functional groups are determined using the infrared Fourier spectrum. The results of the X-ray energy dispersion confirm the correspondence of the ratio of the number of atoms of each material to the nominal stoichiometry. The basic magnetic properties of the obtained and annealed samples are investigated at room temperature using the vibrating spectrum magnetometry (VSM).