Email this article Synthesis of Mg(Fe0.8Ga0.2)2O4 by Gel Combustion Using Glycine and Starch
- Authors: Smirnova M.N.1, Kop’eva M.A.1, Beresnev E.N.1, Goeva L.V.1, Simonenko N.P.1, Nikiforova G.E.1, Trukhanov A.V.2, Ketsko V.A.1
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Affiliations:
- Kurnakov Institute of General and Inorganic Chemistry
- Scientific and Practical Materials Research Center
- Issue: Vol 63, No 10 (2018)
- Pages: 1257-1261
- Section: Synthesis and Properties of Inorganic Compounds
- URL: https://bakhtiniada.ru/0036-0236/article/view/169005
- DOI: https://doi.org/10.1134/S0036023618100182
- ID: 169005
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Abstract
A powdery material Mg(Fe0.8Ga0.2)2O4 has been prepared by combusting a gel containing magnesium(II), iron(III), and gallium(III) nitrates and a glycine–starch mixture. The gel produced during the synthesis has been studied by thermal analysis (TGA/DSC) and IR spectroscopy. This mixture has been shown to be efficient to produce a homogeneous nanosized powderlike material Mg(Fe0.8Ga0.2)2O4. The morphology and properties of ceramic samples are characterized by scanning electron microscopy, X-ray powder diffraction, neutron diffraction, and vibrational magnetometry.
About the authors
M. N. Smirnova
Kurnakov Institute of General and Inorganic Chemistry
Author for correspondence.
Email: smirnova_macha1989@mail.ru
Russian Federation, Moscow, 119991
M. A. Kop’eva
Kurnakov Institute of General and Inorganic Chemistry
Email: smirnova_macha1989@mail.ru
Russian Federation, Moscow, 119991
E. N. Beresnev
Kurnakov Institute of General and Inorganic Chemistry
Email: smirnova_macha1989@mail.ru
Russian Federation, Moscow, 119991
L. V. Goeva
Kurnakov Institute of General and Inorganic Chemistry
Email: smirnova_macha1989@mail.ru
Russian Federation, Moscow, 119991
N. P. Simonenko
Kurnakov Institute of General and Inorganic Chemistry
Email: smirnova_macha1989@mail.ru
Russian Federation, Moscow, 119991
G. E. Nikiforova
Kurnakov Institute of General and Inorganic Chemistry
Email: smirnova_macha1989@mail.ru
Russian Federation, Moscow, 119991
A. V. Trukhanov
Scientific and Practical Materials Research Center
Email: smirnova_macha1989@mail.ru
Belarus, Minsk, 220072
V. A. Ketsko
Kurnakov Institute of General and Inorganic Chemistry
Email: smirnova_macha1989@mail.ru
Russian Federation, Moscow, 119991
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