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Vol 118, No 12 (2017)

Electrical and Magnetic Properties

Crystal Structure and Magnetic Properties of Dy/Gd Superlattices

Antropov N.O., Kravtsov E.A., Proglyado V.V., Ryabukhina M.V., Ustinov V.V.

Abstract

Epitaxial Dy/Gd superlattices were successfully synthesized using high-vacuum magnetron sputtering and their structural and magnetic properties have been studied. Optimum conditions for the epitaxial growth of rare-earth superlattices by magnetron sputtering (in contrast to the traditional molecular-beam technology), including selected single-crystal substrates and buffer layers, as well as the temperature and growth rate, have been considered. Structural peculiarities and their effect on the magnetic properties of the superlattices that comprise ten or more Dy monolayers, have been analyzed.

Physics of Metals and Metallography. 2017;118(12):1209-1214
pages 1209-1214 views

Correlation between the Hall Resistance and Magnetoresistance in the Mixed State of an Nd2 − xCexCuO4 + δ Electronic Superconductor

Charikova T.B., Shelushinina N.G., Petukhov D.S., Kharus G.I., Petukhova O.E., Ivanov A.A.

Abstract

The Hall resistance and the magnetoresistance in the mixed state of the Nd2 − xCexCuO4 + δ quasi-two-dimensional system near the antiferromagnetic-superconductor (AF-SC) phase transition have been measured at doping levels x = 0.14 and 0.15, and a correlation has been established. This correlation can be analyzed using the following power relationship: ρxy(B) ~ [ρxx (B)]β. It was found that index β varied from 0.94 ± 0.03 in the region of AF and SC coexistence (x = 0.14) to 0.6 ± 0.1 in the SC region with the maximum critical temperature (x = 0.15) at low temperatures and weak magnetic fields. This reduction suggests that the symmetry of carrier pairing changes at the boundary of the transition from the phase of antiferromagnetic ordering and spin density waves to the superconducting phase in the presence of antiferromagnetic spin fluctuations.

Physics of Metals and Metallography. 2017;118(12):1184-1191
pages 1184-1191 views

Control of Low-Field Hysteresis Loop Shift of Spin Valves

Chernyshova T.A., Milyaev M.A., Naumova L.I., Proglyado V.V., Maksimova I.K., Pavlova A.Y., Blagodatkov D.V., Ustinov V.V.

Abstract

Spin valves that comprise synthetic antiferromagnet as a component of pinned layer and an exchange-coupled ferromagnet/Ru/ferromagnet structure in the free layer have been prepared by magnetron sputtering. Microobjects have been formed from spin valves by optical and electron-beam lithography. It has been shown that the shift of the low-field magnetoresistance hysteresis loop decreases as the thicknes of the Ru spacer in the free layer of spin valve increases. The almost hysteresis-free odd-field dependences of the magnetoresistance were obtained for micron-sized samples; in this case, the sensitivity is 0.2%/Oe.

Physics of Metals and Metallography. 2017;118(12):1203-1208
pages 1203-1208 views

Nonstationary Dynamics of Vortex-Like Domain Walls in Magnetic Films with In-Plane Anisotropy

Filippov B.N., Dubovik M.N.

Abstract

The dynamic rearrangement of the structure of vortex domain walls (DWs) in films with uniaxial in-plane anisotropy has been examined based on two-dimensional micromagnetic model simulation. The optimum computational region has been chosen; grids with up to 270 × 75 cells 3 nm in size have been used. The scenarios of dynamic rearrangement of the DW structure in strong fields (up to 450 Oe) and in films with thicknesses exceeding 100 nm have been revealed for the first time. The emergence of multivortex instantaneous distributions of magnetization upon an increase in the film thickness and the external field intensity have been established. The dependence of the critical field on the film thickness has been refined.

Physics of Metals and Metallography. 2017;118(12):1192-1202
pages 1192-1202 views

Influence of a Polymer Coating and the Compacting Pressure on the Magnetic Properties of Cobalt-Based Amorphous Alloys

Skulkina N.A., Ivanov O.A., Mazeeva A.K., Kuznetsov P.A., Stepanova E.A., Blinova O.V., Mikhalitsyna E.A., Denisov N.D., Chekis V.I.

Abstract

The influence of a polymer coating applied in the manufacture of magnetic shields on magnetic properties has been studied based on the example of ribbons of a cobalt-based soft magnetic alloy (Co-Fe-Ni-Cr-Mn-Si-B) with the saturation magnetostriction close to zero. The influence of polymer coating has been separated from the effect of the compacting pressure applied upon its formation. The polymer coating was formed on the ribbon in the states with different signs of the saturation magnetostriction. It has been shown that the compacting pressure and the polymer coating have opposite effects on the properties of the ribbon and that these impacts partly level off upon the formation of the coating. The degree of the influence of the polymer coating on the magnetic properties depends on the state of the ribbon and on the sign of the saturation magnetostriction in this state.

Physics of Metals and Metallography. 2017;118(12):1176-1183
pages 1176-1183 views

Structure, Phase Transformations, and Diffusion

Effect of Plastic Deformation on the Formation of the YBa2Cu3Oy Structure

Kuznetsova E.I., Krinitsina T.P., Bobylev I.B., Zyuzeva N.A., Degtyarev M.V.

Abstract

The structure of the YBa2Cu3Oy (123) compound has been investigated after severe plastic deformation by high-pressure torsion performed at room temperature. Distinctive structural features of the samples prepared by standard synthesis and the samples (with increased critical current density) after treatment at t = 200°C in water-saturated atmosphere have been revealed. It has been shown that a lamellar textured structure formed during the annealing of hydrated and deformed samples includes a superconducting orthorhombic phase with a high oxygen index and residual defects that can serve as pinning centers.

Physics of Metals and Metallography. 2017;118(12):1247-1254
pages 1247-1254 views

Effect of the Conditions of the Nanostructuring Frictional Treatment Process on the Structural and Phase States and the Strengthening of Metastable Austenitic Steel

Makarov A.V., Skorynina P.A., Yurovskikh A.S., Osintseva A.L.

Abstract

The effect of the multiplicity of frictional loading with a sliding synthetic diamond indenter at room temperature in an argon medium and the temperature of loading in the range of −196 to +250°C on the phase composition, fine structure, and micromechanical properties of the surface layer of metastable austenitic chromium-nickel steel has been studied. It has been established that the completeness of the strain-induced martensitic γ → α′ transformation in the surface layer of steel is determined by the loading multiplicity and temperature, as well as the level of strengthening grows with an increase in the frictional loading multiplicity, but weakly depends on the frictional treatment temperature. According to the microindentation data, the characteristics of the surface layer strength and resistance to elastic and plastic deformation are improved with an increase in the frictional loading multiplicity. Frictional treatment by scanning with a synthetic diamond indenter at room and negative temperatures provides high quality for the treated surface with a low roughness parameter (Ra = 80.115 nm), and an increase in the frictional loading temperature to 150–250°C leads to the development of a seizure and growth in Ra to 195–255 nm. Using transmission electron microscopy (TEM), it has been shown that frictional treatment results in the formation of nanocrystalline and fragmented submicrocrystalline structures of strain-induced α′-martensite (at a loading temperature of −196°C) and austenite (at a loading temperature of +250°C) in the surface layer of steel alongside with two-phase martensitic-austenitic structures (at a loading temperature of +20°C).

Physics of Metals and Metallography. 2017;118(12):1225-1235
pages 1225-1235 views

Bimodal Structures of Solids Obtained under Megaplastic Strain

Metlov L.S., Brodova I.G., Tkachenko V.M., Petrova A.N., Shirinkina I.G.

Abstract

The evolution of the defect structure of aluminum alloys of different compositions under megaplastic strain at a high quasi-hydrostatic pressure has been studied. The theoretical analysis and numerical calculation of the evolution of the defect structure of solids (metals) under this impact have been performed within the three-defect model of nonequilibrium evolution thermodynamics. The calculation of defect kinetics shows that the presence of coarse grains submerged into a matrix of fine grains at specified parameters and coefficients leads to the additional generation of dislocations and, as a consequence, to the greater dislocation strengthening of a material.

Physics of Metals and Metallography. 2017;118(12):1255-1261
pages 1255-1261 views

Effect of the Size of Al3(Sc,Zr) Precipitates on the Structure of Multi-Directionally Isothermally Forged Al-Mg-Sc-Zr Alloy

Sitdikov O.S., Avtokratova E.V., Mukhametdinova O.E., Garipova R.N., Markushev M.V.

Abstract

The effect of Al3(Sc,Zr) dispersoids on the evolution of the cast Al-Mg-Sc-Zr alloy structure under multi-directional isothermal forging (MIF) has been investigated. The alloy, which has an equiaxed grain structure with a grain size of ~25 μm and contains dispersoids 5–10 and 20–50 nm in size after onestage (at 360°C for 6 h) and two-stage (360°C for 6 h + 520°C for 1 h) annealing, respectively, was deformed at 325°C (~0.65 Tm) up to cumulative strains of e = 8.4. In the initial stages of MIF, new fine (sub)grains surrounded by low-angle and high-angle boundaries (HABs) were formed near the initial grain boundaries. With increasing strain, the volume fraction and misorientation of these crystallites increased, which led to the replacement of a coarse-grained structure with a fine-grained one with a grain size of ~1.5-2.0 μm. Dynamic recrystallization occurred in accordance to a continuous mechanism and was controlled by the interaction of lattice dislocations and/or (sub)grain boundaries with dispersoids that effectively inhibited the migration of boundaries, as well as the rearrangement of lattice dislocations and their annihilation. The particle size and the density of their distribution significantly affected the parameters of the evolved structure; in an alloy with smaller particles, a structure with a smaller grain size and a larger HAB fraction developed.

Physics of Metals and Metallography. 2017;118(12):1215-1224
pages 1215-1224 views

Microstructure and Physicomechanical Properties of a Cu-8 at % Pd Alloy

Volkov A.Y., Kostina A.E., Volkova E.G., Novikova O.S., Antonov B.D.

Abstract

The evolution of the structure, microhardness, and electrical resistivity has been studied during prolonged low-temperature annealings of the Cu-8 at % Pd alloy. An increase in the microhardness and electrical resistivity after annealings at temperatures of 250 and 300°C has been revealed; the preliminary deformation significantly accelerates and enhances this effect; and the X-ray diffraction patterns remain unchanged and correspond to an fcc solid solution. Using transmission electron microscopy, the state of an atomic short-range order has been detected in the quenched alloy; prolonged annealings of the deformed alloy lead to the formation of microregions of the ordered L12 phase.

Physics of Metals and Metallography. 2017;118(12):1236-1246
pages 1236-1246 views

Theory of Metals

A Physical Model for the Initial Stages of the Fragmentation of Polycrystals in the Process of Developed Plastic Deformation

Rybin V.V., Perevezentsev V.N., Svirina Y.V.

Abstract

The contemporary physical ideas and models that make it possible to answer the question of why polycrystals undergo fragmentation at the stage of developed plastic deformation have been considered and analyzed. It has been demonstrated that fragmentation is an accommodation process that matches microand macrolevels in the development of plastic deformation to each other.

Physics of Metals and Metallography. 2017;118(12):1171-1175
pages 1171-1175 views