Enviar artigo por via de e-mail Structure of a new chelate complex MO2O3(dpm)4
- Autores: Ledneva A.Y.1, Artemkina S.B.1, Stabnikov P.A.1, Yanshole L.V.2, Fedorov V.E.1
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Afiliações:
- Nikolaev Institute of Inorganic Chemistry, Siberian Branch
- International Tomography Center, Siberian Branch
- Edição: Volume 58, Nº 4 (2017)
- Páginas: 758-762
- Seção: Article
- URL: https://bakhtiniada.ru/0022-4766/article/view/161420
- DOI: https://doi.org/10.1134/S0022476617040163
- ID: 161420
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Resumo
A new Mo2O3(dpm)4 compound (I) is synthesized by the interaction of Mo(CO)6 with 2,2,6,6-tetramethylheptanedione-3,5 (dpm). The structure of complex I determined by the XRD method is as follows: triclinic crystal system, space group P–1, a = 10.1780(7) Å, b = 10.1817(6) Å, c = 13.3255(9) Å, α = 110.562(2)°, β = 102.233(2)°, γ = 93.9041(19)°, V = 1248.17(14) Å3. The compound is characterized by IR spectroscopy, mass-spectrometry and thermogravimetric analysis (TGA).
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Sobre autores
A. Ledneva
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Autor responsável pela correspondência
Email: ledneva@niic.nsc.ru
Rússia, Novosibirsk
S. Artemkina
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Email: ledneva@niic.nsc.ru
Rússia, Novosibirsk
P. Stabnikov
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Email: ledneva@niic.nsc.ru
Rússia, Novosibirsk
L. Yanshole
International Tomography Center, Siberian Branch
Email: ledneva@niic.nsc.ru
Rússia, Novosibirsk
V. Fedorov
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Email: ledneva@niic.nsc.ru
Rússia, Novosibirsk
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