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Vol 60, No 6 (2017)

Nuclear Experimental Technique

A neutron detector that is insensitive to attendant γ rays

Yakovlev M.V.

Abstract

A neutron detector is described, whose operating principle is based on detecting charge-transfer effects of secondary recoil protons produced in hydrogen-containing materials under exposure to primary neutrons. The physical mechanism of the operation of this detector is presented and its sensitivity is determined as a function of the neutron energy. The design of a detector that is insensitive to attendant γ rays is proposed. The serviceability of the detector has been confirmed experimentally. The detector may find application to tests in mixed fields of γ rays and neutrons.

Instruments and Experimental Techniques. 2017;60(6):771-774
pages 771-774 views

Use of 44Ti in the time-differential γγ perturbed-angular- correlation method for studying condensed matter

Budzinsky M.Z., Velichkov A.I., Karaivanov D.V., Kochetov O.I., Salamatin A.V., Filosofov D.V.

Abstract

The principal aspects of 44Ti application in time-differential γγ perturbed-angular-correlation method (TDPAC) for studying condensed matter are discussed. In the presented spectrometer modification, the efficiency of 44Ti application can be considerably increased by using thin NaI scintillator crystals. Promising techniques for 44Ti production and a method for synthesizing samples are described. Examples of TDPAC studies of titanium (rutile TiO2) and scandium (Sc2O3) oxide samples are shown.

Instruments and Experimental Techniques. 2017;60(6):775-781
pages 775-781 views

Purification of liquid xenon with the spark discharge technique for use in two-phase emission detectors

Akimov D.Y., Belov V.A., Berdnikova A.K., Bobkov S.V., Bolozdynya A.I., Dolgolenko A.G., Dzhumaev P.S., Gusakov Y.V., Guss D.V., Khromov A.V., Kolpakov M.Y., Konovalov A.M., Kovalenko A.G., Kozlova E.S., Krakhmalova T.D., Kumpan A.V., Lukyashin A.V., Melikyan Y.A., Nepochataya O.E., Rudik D.G., Savinov M.Y., Shakirov A.V., Sidorenko A.V., Simakov G.E., Sosnovtsev V.V., Taer G.S.

Abstract

A procedure for spark-discharge purification of a liquid xenon sample with a mass of 55 kg is described. The average lifetime of ionization electrons before capture by electronegative impurities in liquid xenon increased from ≤ 0.1 μs to ≥ 50 μs for an electric field of 50–500 V/cm as a result of the procedure. The xenon purified with this method is intended for use in the RED-100 detector for observation of the process of coherent elastic neutrino scattering off xenon nuclei.

Instruments and Experimental Techniques. 2017;60(6):782-788
pages 782-788 views

Application of Computers in Experiments

The development of Campbell integration system applied in high particle flux measurement

Wang W., Cao J., Zhou X., Yin Z.

Abstract

Campbell Mode is a method widely used in nuclear signal processing. In this article, we introduce the design of the new system based on the Campbell integration measurement applied in NFM (neutron flux measurement) systems for ITER plasma diagnose. In this article, we introduce a digital particle flux measurement system based on Campbell integration theory. A subsequent series of experiment are conducted to test the digital Campbell system performance, which proves that the Campbell integration system is competent for the plasma diagnose in ITER.

Instruments and Experimental Techniques. 2017;60(6):789-794
pages 789-794 views

A high speed photon counter system for microwave mercury ion frequency standard

Chen Y., Wang M., She L., Liu H., Li J.

Abstract

This report describes a high speed photon counter system for microwave mercury ion frequency standard based on a field programmable gate array (FPGA). A high speed comparator is chosen to convert analog signal to digital pulse. A circuit with low-voltage differential signaling (LVDS) receiver in FPGA is used to capture the rising edges of the pulses. In our experiment, the clock of the Altera FPGA EP4CE10E22C8N is 80 MHz which is easy for logic design, and the de-serialization factor of the LVDS receiver is 8, the measured minimum pulse width that can be correctly captured is about 1.67 ns. As a compact and low-cost module, the photon counter system is used for the microwave mercury ion frequency standard.

Instruments and Experimental Techniques. 2017;60(6):795-799
pages 795-799 views

Application of a specific integrated circuit for readout and analog processing of signals from silicon multiplier arrays

Bocharov Y.I., Butuzov V.A., Simakov A.B.

Abstract

A multichannel integrated circuit intended for readout and analog preprocessing of signals from multielement photodetectors has been designed and evaluated. It is optimized for use with silicon photomultiplier arrays. The chip includes current-signal and voltage-signal processing channels. Except for the front end, all of the channels are identical. Each of them contains a code-controlled current amplifier, an integrator, two digitally controlled variable gain amplifiers, a filter, a peak detector, an output buffer with a level shifter, an amplitude discriminator, two timers, and a control unit. The device is configured and tuned by uploading data via a serial interface. The chip is part of a chipset that also includes a multichannel analog-todigital converter with a buffer memory and voltage reference. This chipset makes it possible to build a fullfeatured multielement photodetector signal-processing system, as well as signal processing systems for multichannel detectors of other types. The integrated circuit is implemented in the 0.35 μm CMOS process. This paper also describes the features of the circuits of the device, analyzes the parameters of several of its basic units, and discusses the test results.

Instruments and Experimental Techniques. 2017;60(6):800-810
pages 800-810 views

Electronics and Radio Engineering

Low-pressure gas-discharge current interrupters in a generator of high-voltage nanosecond pulses with an inductive energy storage

Vereshchagin N.M., Kruglov S.A., Serezhin A.A., Shatilov S.G., Agaltsov K.D., Pavlov M.B.

Abstract

Designs of grid units with slotted and multiple-aperture configurations of holes that allow an increase in the stability of the current-cutoff process and a reduction in the time to turn the device off in a high-voltage pulse generator with an inductive energy storage were created. Compared to a TGI2-500/20 thyratron, these designs made it possible to reduce the time instability of the instant of the current interruption by factors of 2 and 5 for switches with the multiple-aperture and slotted configurations of the grids, respectively. These constructions allowed the minimum time for disabling a device to be reduced by 25%.

Instruments and Experimental Techniques. 2017;60(6):811-817
pages 811-817 views

Control systems of high-voltage transistor switches

Ponomarev A.V., Mamontov Y.I.

Abstract

Control systems of high-voltage transistor switches are described. Possible ways to develop these systems are considered. A control system of the transistors of a high-voltage switch on the basis of a current loop is considered in detail. Signals for turning the transistors on and off arrive to their control boards from their common conductor with bipolar current pulses. A positive pulse turns the transistors on, while a negative pulse turns them off. The time interval between these pulses sets the time during which the switch is in the conducting state. The minimum duration of the conducting state is several microseconds, while the maximum duration is not limited. The results of tests of a switch prototype with an operating voltage of up to 4 kV are presented. The operation of the switch was demonstrated when obtaining rectangular pulses in the microsecond range across a resistive load. We also verified the possibility of forming pulses of damped oscillations at a frequency of 1 MHz by this device. The positive test results make it possible to develop switches for operating voltages of tens of kilovolts using the considered approach.

Instruments and Experimental Techniques. 2017;60(6):818-825
pages 818-825 views

The critical aspects in the design of high-current inductors

Kharlov A.V.

Abstract

High-voltage high-current inductors are important components of power-supply systems that are based on capacitor banks with a high energy capacity. The main aspects of designing high-current inductors that were obtained via numerical simulation are presented. A harmonic analysis was performed to take the influence of eddy currents on the inductance value and mechanical stresses into account. It was shown that the choice of materials significantly influences the parameters of the inductor. Calculations of the stray magnetic field in a quasi-toroidal assembly of inductors were performed. It is shown that the leakage magnetic field in the far-field zone is two orders of magnitude lower for an assembly of four inductors than for one inductor.

Instruments and Experimental Techniques. 2017;60(6):826-832
pages 826-832 views

A cathode unit of a pulse-periodic relativistic magnetron

Vintizenko I.I., Mashchenko A.I., Mityushkina V.Y.

Abstract

The construction of a cathode unit of a pulse-periodic relativistic magnetron that contains an alignment adjuster for axial-symmetric installation of a cathode along the full length of anode block is described. The alignment adjuster makes it possible to rapidly adjust the relativistic magnetron to the maximum output power of microwave radiation. In this case, the process of assembling the device becomes considerably simpler.

Instruments and Experimental Techniques. 2017;60(6):833-836
pages 833-836 views

General Experimental Techniques

An experimental setup for investigation of arc and erosion processes in high-voltage high-current breakers

Budin A.V., Pinchuk M.E., Kuznetsov V.E., Leont’ev V.V., Kurakina N.K.

Abstract

An experimental test setup for investigating arc and erosion processes in gas-filled high-voltage high-current switches is described and some results that were obtained on it are presented. The setup includes a discharge chamber that allows simulation of the process of disconnecting the ring and pin contacts, a capacitive energy storage with a capacitance of 0.11 F and a charging voltage of up to 10 kV, and a remotely controlled gas-supply system. The diagnostic complex includes systems for measuring the discharge current, the voltage across the arc, and the pulse pressure in the chamber, as well as high-speed filming and optical spectroscopy. Experiments with a current amplitude of 30–300 kA can be performed on the test bench. During the first current half-period of 1.0–3.0 ms, the contacts move apart to a distance of 3–4 cm. The arc is cooled via transverse gas blowing at a pressure in the chamber of 0.5–1.5 MPa. A movable contact is displaced due to the pressure of the gas that is pumped into the chamber.

Instruments and Experimental Techniques. 2017;60(6):837-842
pages 837-842 views

A facility for permeation measurements under plasma irradiation

Golubeva A.V., Cherkez D.I., Spitsyn A.V., Yanchenkov S.V.

Abstract

An PIM (magnetic plasma source) experimental facility for investigation of permeation of hydrogen isotopes through the structural and plasma-facing materials, which are used in fusion devices, is described. The facility allows investigation of the hydrogen permeation through metal and porous (carbon and carbon composites) membranes in a temperature range of 290–1000 K during interaction of membranes with gaseous hydrogen (the pressure difference between the membrane sides is up to 0.1 atm) and also under irradiation with microwave plasma with a flux density of up to 3 × 1020 atoms/(m2 s). The permeability of ChS-68 austenitic steel was investigated. The experimental data confirmed the correctness of the operation of the facility and the reliability of the results.

Instruments and Experimental Techniques. 2017;60(6):843-852
pages 843-852 views

A high-current subnanosecond electron accelerator with a gas-filled former

Yuriev A.L., Elyash S.L., Loiko T.V., Pukhov S.P., Nikolaev D.P., Seleznev A.A.

Abstract

A subnanosecond electron accelerator prototype based on the ARSA small-size accelerator with a gas-filled former (nitrogen ~4 MPa) has been developed and studied. The operation principle of the former involves charging of a short storage line and its discharge to a stepped line with an accelerating tube that generates electrons. The recorded electron-beam current pulse length was t0.5 = 0.3 ns, the current amplitude was at least 1.5 kA, and the maximum electron energy was ~850 keV.

Instruments and Experimental Techniques. 2017;60(6):853-857
pages 853-857 views

Measuring the refractive index in a wave excited in water by a laser pulse

Zotov S.D., Kazantsev S.Y., Kudryavtsev E.M., Kuznetsov A.A., Lebedev A.A., Firsov K.N.

Abstract

The problem of measuring the refractive index in a spherical wave using the Toepler method with a two-sectional photodetector is considered. A technique for determining the width and amplitude of a wave perturbation from the measured time dependence of a schlieren signal is presented. It is shown experimentally that when a water surface is irradiated with an HF-laser pulse (the pulse energy is 50 mJ, the duration is 60 ns), an elastic wave with a width of ~2 mm and an amplitude that is inversely proportional to the travelled distance is excited. The minimum recorded value of the refractive-index gradient is ~3 × 10–8 mm–1; the absolute measurement error of the refractive index is 1.5 × 10–8. The obtained sensitivity and accuracy exceed the results that were previously published. The proposed approach is characterized by the extreme simplicity of the equipment, as well as by the easiness of the experimental implementation and processing of the measurement results.

Instruments and Experimental Techniques. 2017;60(6):858-863
pages 858-863 views

Physical Instruments in Ecology, Medicine, and Biology

A device for in-situ layer-by-layer measurements of the physical properties of an ice pack

Lukyanov P.Y., Zheleznyak I.I., Gurulev A.A.

Abstract

A device designed for making microholes in ice packs by steaming along with in-situ determination of the physical properties of ice and collection of liquid samples is described. The total intensity of the light that is scattered in the bulk of the ice mass is reflected from the microhole wall surface, as well as resistivity variations of the liquid formed at the bottom of the microhole during the steaming, are measured in the process of deepening the hole.

Instruments and Experimental Techniques. 2017;60(6):864-867
pages 864-867 views

A data-acquisition and control system for spectral-domain optical coherence tomography with a speed of 91 912 A-scans/s based on a USB 3.0 interface

Terpelov D.A., Ksenofontov S.Y., Gelikonov G.V., Gelikonov V.M., Shilyagin P.A.

Abstract

We describe a system of optical spectrum registration at the output of an interferometer with controlled phase shifts for an experimental device intended for visualizing the internal structure of an optically turbid specimen, using the method of spectral domain optical coherence tomography. A device for spectral domain optical coherence tomography based on a common-path optical scheme with a USB 3.0 interface for inputting data into a computer has been developed. An imaging speed of 91 912 A-scans/s has been attained. At the achieved speed, a series of live experiments were carried out to visualize the internal structure of skin tissues from a finger and front segments of an eye.

Instruments and Experimental Techniques. 2017;60(6):868-874
pages 868-874 views

Laboratory Techniques

A study of the performance of an induction sensor for an accelerator of charged microparticles

Telegin A.M., Piyakov A.V.

Abstract

The design details and parameters of an induction sensor for a linear accelerator that is used to measure the velocity and charge of accelerated particles are described. A theoretical calculation of the voltage picked up from the Faraday cup of the induction sensor versus the particle parameters is presented. The essential feature of this calculation is the fact that the induction-sensor voltage is considered not only as a function of the velocity and charge of a detected charged particle, but also as a function of the coordinate of this particle. The experimental data that characterize the performance of the induction sensor are presented.

Instruments and Experimental Techniques. 2017;60(6):875-879
pages 875-879 views

Adapter modification for a high-speed centrifuge rotor for use with standard medical polypropylene tubes

Atamanov I.V., Aleksenskii A.E., Shvidchenko A.V., Rabchinskii M.K.

Abstract

A rotor adapter for a Sartorius Sigma 3-30KS centrifuge (rotor 12158), which is used for centrifugal separation of detonation nanodiamond particles with different sizes at accelerations of 6 × 104 g, was developed and tested. The developed adapter allows one to use common medical polypropylene test tubes after their simple modification instead of the expensive test tubes that are usually recommended by the manufacturer of the centrifuge. As a result, the use of the adapter significantly decreases expenses on experiments, where fractionation of various liquid dispersions is applied.

Instruments and Experimental Techniques. 2017;60(6):880-882
pages 880-882 views

Determining the kinematic parameters of moving test objects via the results of video recording

Borozenets A.S., Proskurin A.V.

Abstract

Algorithms for processing results of high-speed video recording of the processes of interaction between test objects and barriers are presented. The algorithms make it possible to determine the position of the test object relative to a barrier, as well as the kinematic parameters (the velocity and acceleration) of the points of the test object before, during, and after interaction with the barrier at initial test object collision velocities of up to 120 m/s. The efficiency of the developed algorithms is confirmed by the good coincidence of the results of videogram processing with the results of acceleration measurements by piezoelectric accelerometers.

Instruments and Experimental Techniques. 2017;60(6):883-887
pages 883-887 views

An automatic apparatus for the preparation of thin films by successive ionic layer deposition

Andronov A.O., Matyushkin L.B., Khondryukov D.V., Aleksandrova A.O., Moshnikov V.A.

Abstract

An automatic apparatus for the preparation of thin-film coatings by successive ionic layer deposition is presented. The basic design, engineering, and operating parameters of the apparatus are the specimenpositioning accuracy with respect to the phase boundaries of 10 μm, a substrate speed in the solution of 0.5–3 mm/s, and a temperature range of 25–90°C. The apparatus was tested in the course of preparation of cadmium sulfide thin films from aqueous–alcohol solutions. The resulting specimens had a dense homogeneous surface, a thickness of 1.3–25.5 nm, depending on the number of the layer-deposition cycles, and an energy gap width of 2.3–2.5 eV.

Instruments and Experimental Techniques. 2017;60(6):888-891
pages 888-891 views

An apparatus for vacuum deposition of composite TiN−Cu coatings using coupled vacuum-arc and ion-plasma processes

Semenov A.P., Tsyrenov D.B., Semenova I.A.

Abstract

A plasma-chemical reactor with the coupling of gas-discharge processes has been developed. These processes combine arc evaporation of titanium in a nitrogen-containing plasma and ion-plasma sputtering of copper with the formation of copper vapor. Experiments were carried out on the deposition of superhard nanostructured TiN−Cu composite layers.

Instruments and Experimental Techniques. 2017;60(6):892-895
pages 892-895 views

A photometric method for determining the diffusivity of dyes in aqueous solutions in a thin horizontal cell

Krasnoperov Y.I., Sklyarenko M.S.

Abstract

A photometric method for determining the diffusivity of dyes in aqueous solutions in a thin horizontal cell using a digital camera is proposed. This method simplifies measurements and reduces the measurement time. The photometric technique that is used to determine the diffusivity does not require the construction of a calibration dependence of the brightness on the concentration. A model of the measuring instrument was developed, as well as various designs of measuring cells. The instrument was tested in experiments on measurements of the diffusivity of dyes in water. The relative error of the instrument is below 10%.

Instruments and Experimental Techniques. 2017;60(6):896-901
pages 896-901 views